GB/T 35501-2017 in English
VALIDMethyltrimethoxysilane for industrial use
- Issued on:2017-12-29
- Implemented on:2018-07-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
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《GB/T 35501-2017工业用甲基三甲氧基硅烷》由TC63(全国化学标准化技术委员会)归口,主管部门为中国石油和化学工业联合会。
Introduction
GB/T 35501-2017 Interpretation of the Standard for Industrial Methyltrimethoxysilane
1. Background and Significance of Standard Formulation
Industrial methyltrimethoxysilane (MTMS) is an important chemical product, which is widely used in organic synthesis, electronic materials, coatings and other fields. In order to standardize product quality and technical requirements and ensure its safety and applicability, the national standard GB/T 35501-2017 came into being.
The standard was proposed by the China Petroleum and Chemical Industry Federation and managed by the Organic Chemical Industry Branch of the National Technical Committee for Chemical Standardization, which fully reflects the authority and representativeness of the industry.
2. Scope and applicability of the standard
This standard applies to methyltrimethoxysilane prepared from monomethyltrichlorosilane and methanol through alcoholysis, neutralization and distillation. Its structural formula is:
The relative molecular mass is 136.22, which meets the requirements of international standards.
| Comparison of technical indicators of industrial methyltrimethoxysilane | |||
|---|---|---|---|
| Items | Superior products | First-class products | Qualified products |
| Chroma/Hazen unit (platinum-cobalt color number) | ≤10 | ||
| Methyltrimethoxysilane, w/% | ≥99.5 | ≥99.0 | ≥98.0 |
| Methanol, w/% | |||
| pH value | 3.8~7.0 | ||
| Chloride (as Cl-)/(mg/kg) | ≤50 | ||
3. Quality inspection methods and standard requirements
According to GB/T 35501-2017, the inspection indicators of industrial methyltrimethoxysilane include appearance, colorimetry, content analysis, etc. Among them:
3.1 Application of gas chromatography
Gas chromatograph (with hydrogen flame ionization detector) is used to separate and quantitatively analyze the samples. It is recommended to use a capillary column (dimethylpolysiloxane, 30m×0.32mm×1.0μm), and the typical operating conditions are as follows:
- Vaporization chamber temperature: 250℃
- Detector temperature: 260℃
- Column box temperature: initial 50℃, heating to 180℃ at 20℃/min
During sample handling, care should be taken to avoid contact with air to ensure the accuracy of the analysis results. The mass fraction of each component is calculated by the area normalization method, and the relative deviation of parallel determinations should be controlled within the specified range.
4. Safety and Protection Recommendations
Methyltrimethoxysilane is dangerous to a certain extent. Its flash point is 11°C and its vapor and air can form an explosive mixture. Users should:
- Keep away from open flames and high temperature areas
- Wear protective equipment (such as gloves, goggles)
- Ensure good ventilation and avoid prolonged contact
5. Implementation suggestions and precautions
To ensure that product quality meets the requirements of GB/T 35501-2017, manufacturers should:
- Strictly control the quality of raw materials
- Optimize production process
- Perform regular type inspection (at least once every 6 months)
- Strengthen employee training to ensure that operations comply with safety regulations
Conclusion:GB/T 35501-2017 provides a scientific basis for the quality control of industrial methyltrimethoxysilane. By strictly following the standard requirements and test methods, product quality can be effectively guaranteed and meet the needs of downstream application fields.

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