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volatile organic compounds residues headspace gas chromatography-mass spectrometry headspace gas chromatography-mass spectrometry residual volatile organic compounds independent characteristics detection principle headspace gas chromatography-mass spectrometry us standards key parameters headspace temperature thickness — microscopical method gb/t space high-energy astronomical radiation sources gb/t23694 risk management terminology
GB/T 35862-2018 in English

GB/T 35862-2018 in English

VALID

Surface active agents—Determination of volatile organic compounds residues—Headspace gas chromatography-mass spectrometry (GC-MS)

  • Issued on:2018-02-06
  • Implemented on:2018-09-01
  • File Format:PDF
  • Delivery:Via email within 1~3 business days
Price(USD): $70.00
$68.00
Standard No: GB/T 35862-2018
Document status: VALID
Title in English: Surface active agents—Determination of volatile organic compounds residues—Headspace gas chromatography-mass spectrometry (GC-MS)
Title in Chinese: 表面活性剂 挥发性有机化合物残留量的测定 顶空气相色谱质谱(GC-MS)联用法
Language: English
File Format: Electronic (PDF)
Delivery: Via email within 1~3 business days
Issued on: 2018-02-06
Implemented on: 2018-09-01
Chinese Classification: G72-Basic standards and general methods for surface active agent
Professional Classification: GB-National Standard
Related Keywords: volatile organic compounds residues headspace gas chromatography-mass spectrometry
headspace gas chromatography-mass spectrometry
residual volatile organic compounds
independent characteristics detection principle headspace gas chromatography-mass spectrometry
us standards key parameters headspace temperature
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GB/T 35862-2018
Determination of total volatile substances by gas phase
Temperamental Headspace Repeatability
Organic amine content gas chromatography mass spectrometry
The gas phase headspace method sometimes has peaks and sometimes no peaks

《GB/T 35862-2018表面活性剂 挥发性有机化合物残留量的测定 顶空气相色谱质谱(GC-MS)联用法》由TC63(全国化学标准化技术委员会)归口,TC63SC8(全国化学标准化技术委员会(特种)界面活性剂分会)执行,主管部门为中国石油和化学工业联合会。


Introduction

1. Background and significance of the standard

GB/T 35862-2018 "Determination of residual volatile organic compounds in surfactants - Headspace gas chromatography-mass spectrometry (GC-MS) method" is an important national standard used to regulate the detection method of residual volatile organic compounds (VOCs) in surfactants. With the enhancement of environmental awareness and the improvement of product quality requirements, the formulation of this standard provides a scientific and unified technical basis for the industry.

2. Comparison of standard frameworks

Chapter Contents GB/T 35862-2018 Comparison with international standards Differences in industry standards
Scope and Applicability Applicable to the determination of VOC residues in various surfactants In line with international standards such as ISO 16000 series Meet domestic industry needs and have independent characteristics
Detection Principle Headspace Gas Chromatography-Mass Spectrometry (GC-MS) International General Method Consistent with EU and US standards
Key parameters Headspace temperature: 80±1℃, equilibration time 40 minutes International standard recommended range 30-60 minutes Domestic standards are more operational

3. Standard implementation recommendations

3.1 Laboratory conditions requirements

Hardware facilities:Equipped with headspace gas chromatography-mass spectrometry (GC-MS), headspace injector and other equipment to ensure that the laboratory environment meets the temperature and humidity control requirements.

Staff capabilities:Testers must undergo professional training and be familiar with GC-MS operating procedures and data processing methods.

3.2 Sample preparation and processing

In practical applications, it is recommended to weigh samples strictly in accordance with standard requirements and ensure that the headspace bottle is well sealed. For samples with higher volatility, the sampling volume can be appropriately reduced to avoid detection errors.

3.3 Data analysis and quality control

When establishing a standard curve, it is necessary to ensure that the linear relationship between each concentration point is good (the correlation coefficient should be greater than 0.99). For precision requirements, the relative deviation of two measurement results by the same operator should be less than 10%.

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