GB/T 35862-2018 in English
VALIDSurface active agents—Determination of volatile organic compounds residues—Headspace gas chromatography-mass spectrometry (GC-MS)
- Issued on:2018-02-06
- Implemented on:2018-09-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$68.00
《GB/T 35862-2018表面活性剂 挥发性有机化合物残留量的测定 顶空气相色谱质谱(GC-MS)联用法》由TC63(全国化学标准化技术委员会)归口,TC63SC8(全国化学标准化技术委员会(特种)界面活性剂分会)执行,主管部门为中国石油和化学工业联合会。
Introduction
1. Background and significance of the standard
GB/T 35862-2018 "Determination of residual volatile organic compounds in surfactants - Headspace gas chromatography-mass spectrometry (GC-MS) method" is an important national standard used to regulate the detection method of residual volatile organic compounds (VOCs) in surfactants. With the enhancement of environmental awareness and the improvement of product quality requirements, the formulation of this standard provides a scientific and unified technical basis for the industry.
2. Comparison of standard frameworks
| Chapter Contents | GB/T 35862-2018 | Comparison with international standards | Differences in industry standards |
|---|---|---|---|
| Scope and Applicability | Applicable to the determination of VOC residues in various surfactants | In line with international standards such as ISO 16000 series | Meet domestic industry needs and have independent characteristics |
| Detection Principle | Headspace Gas Chromatography-Mass Spectrometry (GC-MS) | International General Method | Consistent with EU and US standards |
| Key parameters | Headspace temperature: 80±1℃, equilibration time 40 minutes | International standard recommended range 30-60 minutes | Domestic standards are more operational |
3. Standard implementation recommendations
3.1 Laboratory conditions requirements
Hardware facilities:Equipped with headspace gas chromatography-mass spectrometry (GC-MS), headspace injector and other equipment to ensure that the laboratory environment meets the temperature and humidity control requirements.
Staff capabilities:Testers must undergo professional training and be familiar with GC-MS operating procedures and data processing methods.
3.2 Sample preparation and processing
In practical applications, it is recommended to weigh samples strictly in accordance with standard requirements and ensure that the headspace bottle is well sealed. For samples with higher volatility, the sampling volume can be appropriately reduced to avoid detection errors.
3.3 Data analysis and quality control
When establishing a standard curve, it is necessary to ensure that the linear relationship between each concentration point is good (the correlation coefficient should be greater than 0.99). For precision requirements, the relative deviation of two measurement results by the same operator should be less than 10%.

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