GB/T 36592-2018 in English
VALIDMethods for chemical analysis of rhodium—Determination of platinum,ruthenium,iridium,palladium,gold,silver,copper,iron,nickel,aluminum,lead,manganese,magnesium,tin,zinc,silicon contents—Inductively coupled plasma mass spectrometry
- Issued on:2018-09-17
- Implemented on:2019-06-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$156.00
| Standard No: | GB/T 36592-2018 |
| Document status: | VALID |
| Title in English: | Methods for chemical analysis of rhodium—Determination of platinum,ruthenium,iridium,palladium,gold,silver,copper,iron,nickel,aluminum,lead,manganese,magnesium,tin,zinc,silicon contents—Inductively coupled plasma mass spectrometry |
| Title in Chinese: | 铑粉化学分析方法 铂、钌、铱、钯、金、银、铜、铁、镍、铝、铅、锰、镁、锡、锌、硅的测定 电感耦合等离子体质谱法 |
| Language: | English |
| File Format: | Electronic (PDF) |
| Delivery: | Via email within 1~3 business days |
| Issued on: | 2018-09-17 |
| Implemented on: | 2019-06-01 |
| ICS Classification: | 77.120.99-Other non-ferrous metals and their alloys |
| Chinese Classification: | H15-Precious metals and its alloy analysis method |
| Professional Classification: | GB-National Standard |
| Related Keywords: | plasma mass spectrometry
plasma mass spectrometry introduction chemical analysis methods standard frameworks dimension range detection limit internal standard platinum rhodium determination |
| Related Topics: | Ferro Ruthenium Separation
Palladium Ruthenium Alloy Nano GB/T 36592-2018 gb/t+36592 Chemical analysis method of iridium powder GBT36592 GB/T 36592-2018 Method for masking metal cations iron, magnesium and aluminum Ruthenium powder general quality Magnesium metal quality |
《GB/T 36592-2018铑粉化学分析方法 铂、钌、铱、钯、金、银、铜、铁、镍、铝、铅、锰、镁、锡、锌、硅的测定 电感耦合等离子体质谱法》由TC243(全国有色金属标准化技术委员会)归口,TC243SC5(全国有色金属标准化技术委员会贵金属分会)执行,主管部门为中国有色金属工业协会。
Introduction
1. Standard Overview
GB/T 36592-2018 "Chemical Analysis Methods for Powder - Determination of Platinum, Ruthenium, Iridium, Palladium, Gold, Silver, Copper, Iron, Nickel, Aluminum, Lead, Manganese, Magnesium, Tin, Zinc and Silicon - Inductively Coupled Plasma Mass Spectrometry" is a national standard proposed by the China Nonferrous Metals Industry Association, mainly for the determination of various metal elements in powder.
2. Principle of the Method
This standard adopts inductively coupled plasma mass spectrometry (ICP-MS) to quantitatively analyze platinum (Pt), Ruthenium (Ru), Iridium (Ir), Palladium (Pd), Gold (Au), Silver (Ag) and other elements in the sample by internal standard method. The specific steps include sample dissolution, sample processing and signal determination.
3. Comparison of Standard Frameworks
| Dimension | Range | Detection Limit | Internal Standard |
|---|---|---|---|
| Platinum (Pt) | 0.000 05~0.050% | 0.1 ng/mL | No Internal Standard |
| Iridium (Ir) | 0.000 05~0.050% | 0.1 ng/mL | No Internal Standard |
| Palladium (Pd) | 0.000 05~0.050% | 0.1 ng/mL | Yttrium internal standard |
4. Implementation suggestions
In actual applications, it is recommended that operators strictly follow the standard requirements for sample pretreatment and pay attention to the following points:
- Ensure that the purity of the reagents used reaches the MOS level.
- The instrument operating parameters should comply with the recommended values in Table A.1.
- Regularly calibrate the instrument to ensure that the linear correlation coefficient is ≥0.9995.

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