SN/T 3184-2012 in English

VALID

Food contact materials-Polymers-Determination of bis (hydroxyphenyl) methane bis (2,3-epoxypropyl) ethers in food simulants-Gas chromatography-mass spectrometry

Issued on:2012-05-07
Implemented on:2012-11-16
File Format:PDF
Delivery:Via email within 1~3 business days

Price(USD)： $160.00
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Standard No:	SN/T 3184-2012
Document status:	VALID
Title in English:	Food contact materials-Polymers-Determination of bis (hydroxyphenyl) methane bis (2,3-epoxypropyl) ethers in food simulants-Gas chromatography-mass spectrometry
Title in Chinese:	食品接触材料高分子材料食品模拟物中双（羟苯基）甲烷-双（2，3-环氧丙基）醚的测定气相色谱-质谱法
Language:	English
File Format:	Electronic (PDF)
Delivery:	Via email within 1~3 business days
Issued on:	2012-05-07
Implemented on:	2012-11-16
Professional Classification:	SN-Import&Export Inspection
Related Keywords:	gas chromatography-mass spectrometry simulants-gas chromatography-mass spectrometry introduction interpretation food simulants methane bis mass spectrometry
Related Topics:	food contact material sn/t+3438-2012 Efficient Dioxygen Molecule sn/t+3367-2012 dual gas phase magnetic mass spectrometry Epoxy polymer material sn/t3367-2012 Shuangjiazi Chromatographic bifid food contact material Chromatographic material Hydroxylation Mass Spectrometry food grade hydrogen peroxide How to Simulate Mass Spectrometry Chromatography Simulation GC-MS gas phase of polymer Chromatographic polymer materials food grade hydrogen peroxide Dual fid chromatography Hydroxyl Mass Positive food simulants sn material Hydroxylation Mass Spectrometry gas phase bimolecule sn/t3395-2012 dual tube mass spectrometry Hydroxyl in mass spectrum food simulants food simulation dual mass mode Chromatographic material Mass Spectrometry Food Packaging Materials Mass Spectrometry Food Contact Materials Mass spectrum baseline is too high mass spectrum Gas Chromatography Dual Column Dual Detector Principle How to deal with high mass spectrum baseline Contact angle measurement of carbon-based materials food materials sn/t 2012

Introduction

Interpretation of the core content of the standard

This standard specifies the detection method for BFDGE in water-based (3% acetic acid, 10% ethanol) and fat-based (isooctane) food simulants, using gas chromatography-mass spectrometry as the main analytical equipment, and the method detection limit is 0.05 mg/L.

Comparison of key technologies

Detection elements	Water-based simulants	Lipid-based simulants
Pretreatment method	HLB solid phase extraction purification	Direct nitrogen concentration
Recovery solvent	Tetrahydrofuran	Tetrahydrofuran
Key parameters	Column flow rate ≤1 mL/min	50℃ water bath nitrogen blowing

Detailed explanation of instrument parameters

The standard recommended DB-5MS chromatographic column (30m×0.25mm×0.25μm) must meet the following conditions:

Program temperature: 150℃(2min)→270℃(30℃/min)→hold for 7min
Selected ion monitoring (SIM): m/z 181 (quantitative ion), 197/312 (qualitative ion)
Carrier gas flow rate: 1.0 mL/min (high-purity nitrogen)

Key points for standard implementation

Preparation of standard: The stock solution (5mg/mL) must be stored at 4℃ away from light, with a validity period of 3 months
Quality control: standard curve correlation coefficient ≥ 0.996, parallel sample relative deviation ≤ 10%
Interference elimination: blank simulant must be processed simultaneously for background subtraction

Technology evolution analysis

When this standard was issued in 2012, it first established a dedicated detection method for BFDGE. Compared with EU Directive 2002/72/EC, it adds:

Applicability of isooctane simulant
Solid phase extraction cleanup steps
Defined mass spectrometry qualitative and quantitative ion pairs

More samples: QC/T 942-2021 JGJ 94-2008 NB/T 47013.2-2015

Sample only — not a preview of SN/T 3184-2012

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