GB/T 23673-2019 in English
VALID3,4-Dichloroaniline
- Issued on:2019-12-31
- Implemented on:2020-11-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$156.00
《GB/T 23673-20193,4-二氯苯胺》由TC134(全国染料标准化技术委员会)归口,主管部门为中国石油和化学工业联合会。
Introduction
GB/T 23673-2019 Standard Overview
GB/T 23673-2019 "3,4-Dichloroaniline" is the latest national standard formulated by China for this chemical, replacing the original GB/T 23673-2009 version. This standard mainly specifies the quality requirements, test methods and safety information of 3,4-dichloroaniline.
Comparison of standard frameworks
| Project dimensions | GB/T 23673—2019 | Main changes compared with GB/T 23673—2009 |
|---|---|---|
| Scope of application of the standard | Applicable to quality control of 3,4-dichloroaniline products | Added provisions on the allowable difference in net content of packaging |
| Quality requirements | Table 1 specifies the requirements for appearance, initial melting point, purity and other indicators | The p-chloroaniline content indicator of superior products has been modified, and the allowable difference requirement for moisture determination has been added |
| Test methods | Purity and organic impurity content determination by gas chromatography | Added the accuracy requirement of analytical balance (0.1mg) and specific specifications for water content determination |
Key technology interpretation
Application of gas chromatography:In Section 6.4, the standard specifies the use of capillary column and hydrogen flame ionization detector (FID) to determine the purity and organic impurities of 3,4-dichloroaniline. This method uses the peak area normalization method for quantification, ensuring the accuracy of the analysis results.
Importance of water content determination:The standard adds specific requirements and determination methods for water content (Section 6.5). Weigh about 2.0g of the sample and dissolve it in a mixed solvent of chloroform and methanol for determination. The absolute value of the difference between the two parallel determination results should not exceed 0.05%.
Implementation Suggestions
1. In the actual production process, enterprises should strictly follow the standard requirements to conduct product quality inspection and packaging label management.
2. When using gas chromatograph, it is necessary to calibrate the equipment regularly and ensure that the purity of the reagents meets the requirements.
3. In terms of safety, it is recommended that enterprises strengthen employee protection training and strictly follow the regulations on the storage and transportation of hazardous chemicals.

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