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migratable fluorescent migratable fluorescent brighteners qualitative determination method qualitative determination board determination several specific fluorescent key-value cloud data management application interfaces y-shaped stainless steel heating applications
GB/T 27741-2018 in English

GB/T 27741-2018 in English

VALID

Paper and board—Determination of migratable fluorescent whitening agents

  • Issued on:2018-12-28
  • Implemented on:2019-07-01
  • File Format:PDF
  • Delivery:Via email within 1~3 business days
Price(USD): $120.00
$117.00
Standard No: GB/T 27741-2018
Document status: VALID
Title in English: Paper and board—Determination of migratable fluorescent whitening agents
Title in Chinese: 纸和纸板 可迁移性荧光增白剂的测定
Language: English
File Format: Electronic (PDF)
Delivery: Via email within 1~3 business days
Issued on: 2018-12-28
Implemented on: 2019-07-01
Superseding: GB/T 27741-2011 paper and board - determination of migratable fluorescent whitening agents
Chinese Classification: Y30-Papermaking in general
Professional Classification: GB-National Standard
Related Keywords: migratable fluorescent
migratable fluorescent brighteners
qualitative determination method qualitative determination
board determination
several specific fluorescent
Related Topics: Fluorescent whitening agent
Fluorescence standard plate
Fluorescence standard plate
Standard phosphor plate
Standard phosphor plate
Fluorescent plate
Fluorescent German
Four pole migration
brightener
Migratable optical brightener
Paper fluorescent agent
Fluorescence detection plate
System Board Fluorescence
Trigger fluorescence
rhodium migration
Phenomenal fluorescence
fluorescent paper
plate time fluorescence
plasticizer migration
Fluorescent plate plate
fluorescent version
Fluorescent agent performance
gb27741
GBT27741
GB/T 27741-2011
GB/T 27741-2018
Paper fluorescent agent standard range
Poor reproducibility of fluorescence quantification
Migration test
Pulp coloring and whitening
Fluorescent whitening agent testing standards and basis
Detection of Migrating Fluorescent Whitening Agents
Fluorescent agent detection on drawing paper
Dialysis paper fluorescence test reference
Migration resistance test
gb/t 27741
gbt27741-2018

《GB/T 27741-2018纸和纸板 可迁移性荧光增白剂的测定》由TC141(全国造纸工业标准化技术委员会)归口,主管部门为中国轻工业联合会。


Introduction

Background and significance of the revision of GB/T 27741-2018

The GB/T 27741 series of standards are mainly used to determine the content of migratable fluorescent brighteners in paper and paperboard. The latest version (GB/T 27741-2018) has been significantly revised and improved in many aspects. This revision not only updates the scope of application and definition clauses, but also adds key indicators such as detection limit and recovery rate, further improving the scientificity and practicality of the standard.

Analysis of qualitative determination method

Qualitative determination mainly determines whether the sample contains migratable fluorescent brighteners by fluorescence phenomenon under ultraviolet light. The specific steps include:

  1. Sample preparation: Cut the paper into small pieces and mix them evenly.
  2. Extraction and filtration: Use an extraction solution adjusted to a specific pH value for extraction and filter through a glass funnel.
  3. Gauze adsorption: immerse the filtrate under ultraviolet light to observe the fluorescence phenomenon.

Comparison of quantitative determination methods

Method name Principle overview Scope of application Sensitivity
UV-visible spectrophotometry By measuring the absorbance, a standard curve is established for quantitative analysis. Applicable to most paper and paperboard samples, but easily interfered by other substances. Detection limit: 20.0 mg/kg
High performance liquid chromatography Qualitative and quantitative analysis is performed using HPLC technology combined with a fluorescence detector. Several specific fluorescent whitening agents can be determined simultaneously with accurate results. Detection limit: 1.0 mg/kg

Main changes in the revision of the standard

Comparison between the old and new standards:

  • Scope of application: The new standard expands the detection requirements for migratable fluorescent whitening agents in pulp.
  • Definition of terms: The migration characteristics of "migratable fluorescent whitening agents" under specific conditions are clearly defined.
  • New equipment: Key instruments such as a constant temperature oscillating water bath and a high performance liquid chromatograph are introduced.
  • Data requirements: The detection limit and recovery rate indicators are added to improve the reliability of the test results.

Implementation suggestions

Laboratory operation suggestions:

  1. Choose the appropriate determination method (spectrophotometry or HPLC) according to the sample type.
  2. Strictly control the pH value of the extract to ensure that the experimental conditions meet the standard requirements.
  3. Regularly calibrate the instruments to ensure the accuracy of the test results.
  4. Pay attention to personal protection to avoid potential harm to operators from fluorescent whitening agents.

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