GB/T 27741-2018 in English
VALIDPaper and board—Determination of migratable fluorescent whitening agents
- Issued on:2018-12-28
- Implemented on:2019-07-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$117.00
《GB/T 27741-2018纸和纸板 可迁移性荧光增白剂的测定》由TC141(全国造纸工业标准化技术委员会)归口,主管部门为中国轻工业联合会。
Introduction
Background and significance of the revision of GB/T 27741-2018
The GB/T 27741 series of standards are mainly used to determine the content of migratable fluorescent brighteners in paper and paperboard. The latest version (GB/T 27741-2018) has been significantly revised and improved in many aspects. This revision not only updates the scope of application and definition clauses, but also adds key indicators such as detection limit and recovery rate, further improving the scientificity and practicality of the standard.
Analysis of qualitative determination method
Qualitative determination mainly determines whether the sample contains migratable fluorescent brighteners by fluorescence phenomenon under ultraviolet light. The specific steps include:
- Sample preparation: Cut the paper into small pieces and mix them evenly.
- Extraction and filtration: Use an extraction solution adjusted to a specific pH value for extraction and filter through a glass funnel.
- Gauze adsorption: immerse the filtrate under ultraviolet light to observe the fluorescence phenomenon.
Comparison of quantitative determination methods
| Method name | Principle overview | Scope of application | Sensitivity |
|---|---|---|---|
| UV-visible spectrophotometry | By measuring the absorbance, a standard curve is established for quantitative analysis. | Applicable to most paper and paperboard samples, but easily interfered by other substances. | Detection limit: 20.0 mg/kg |
| High performance liquid chromatography | Qualitative and quantitative analysis is performed using HPLC technology combined with a fluorescence detector. | Several specific fluorescent whitening agents can be determined simultaneously with accurate results. | Detection limit: 1.0 mg/kg |
Main changes in the revision of the standard
Comparison between the old and new standards:
- Scope of application: The new standard expands the detection requirements for migratable fluorescent whitening agents in pulp.
- Definition of terms: The migration characteristics of "migratable fluorescent whitening agents" under specific conditions are clearly defined.
- New equipment: Key instruments such as a constant temperature oscillating water bath and a high performance liquid chromatograph are introduced.
- Data requirements: The detection limit and recovery rate indicators are added to improve the reliability of the test results.
Implementation suggestions
Laboratory operation suggestions:
- Choose the appropriate determination method (spectrophotometry or HPLC) according to the sample type.
- Strictly control the pH value of the extract to ensure that the experimental conditions meet the standard requirements.
- Regularly calibrate the instruments to ensure the accuracy of the test results.
- Pay attention to personal protection to avoid potential harm to operators from fluorescent whitening agents.

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