GB/T 32669-2016 in English
VALIDExtinction spectra characterization of aggregate structure of gold nanorods
- Issued on:2016-04-25
- Implemented on:2016-11-01
- File Format:PDF
- Delivery:Within 1 day
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《GB/T 32669-2016金纳米棒聚集体结构的消光光谱表征》由TC279(全国纳米技术标准化技术委员会)归口,主管部门为中国科学院。
Introduction
1. Scope of the standard and normative references
This standard specifies a method for characterizing the structure of gold nanorod aggregates based on extinction spectroscopy, which is applicable to the characterization of gold nanorods and other precious metal nanoaggregates. The main references include GB/T13966, GB/T19619 and GB/T24369.1-2009.
2. Background of standard formulation
Due to their unique optical properties, gold nanorods have important application value in the fields of biological detection and imaging. However, there is no unified standard for the influence of their aggregate structure on the surface plasmon resonance characteristics. This standard is based on extinction spectroscopy and fills the gap in related fields at home and abroad.
3. Comparison of standard frameworks
| Dimensions | This standard | International standard | Industry standard |
|---|---|---|---|
| Scope of application | Gold nanorod aggregates | Noble metal nanomaterials | Other nanostructures |
| Core methods | Extinction spectroscopy | Scattering and imaging technology | Combination of multiple characterization methods |
| Parameter calculation | Agglomeration parameter AI | Particle size distribution analysis | Dispersion evaluation |
4. Analysis of technology evolution
From spherical gold particles to rod-shaped nanostructures, the study of surface plasmon resonance characteristics has undergone a transition from simple size effects to complex arrangements. This standard achieves quantitative evaluation of aggregate structures based on the extinction spectrum characteristics of EE and SS assemblies.
5. Implementation recommendations
Case analysis: EE and SS assembly characterization
EE and SS assemblies of gold nanorods were tested by UV/visible/near-infrared extinction spectroscopy. The experimental results show that the long-wavelength plasmon resonance peak is red-shifted in the EE mode, while it is blue-shifted in the SS mode. This shows that the arrangement of aggregates has a significant effect on the optical properties.
Specific implementation suggestions include:
- Ensure instrument calibration (e.g. Cary UV/Vis spectrophotometer)
- Control sample concentration to maintain extinction between 0.2 and 0.9
- Perform multiple measurements and average to reduce error

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