GB/T 33426-2016 in English
VALIDRubber shoes--Determination of organotin compounds
- Issued on:2016-12-30
- Implemented on:2017-07-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
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《GB/T 33426-2016胶鞋 有机锡化合物含量试验方法》由TC35(全国橡胶与橡胶制品标准化技术委员会)归口,TC35SC9(全国橡胶与橡胶制品标准化技术委员会胶鞋分会)执行,主管部门为中国石油和化学工业联合会。
Introduction
1. Background and significance of the standard
GB/T 33426-2016 "Test method for organotin compounds in rubber shoes" is a national standard of the People's Republic of China, used to determine the content of organotin compounds in rubber shoes. The standard was officially implemented on July 1, 2017 and is applicable to all types of rubber shoes such as uppers, linings and insoles.
2. Principle of the method
This method uses gas chromatography-mass spectrometry (GC/MS) technology, tropolone as a complexing agent, combined with ultrasonic extraction and liquid-liquid extraction, to achieve quantitative analysis of organotin compounds. The internal standard method is used for quantification to ensure the accuracy of the test results.
3. Comparison of standard frameworks
| Standard dimensions | GB/T 33426-2016 | Comparison with international standards |
|---|---|---|
| Scope of application | Determination of organotin compounds in rubber shoes materials | In line with internationally accepted methods, applicable to a variety of rubber products |
| Detection limit | 0.2 mg/kg | In line with ISO standard requirements |
| Analysis time | About 60 minutes/sample | On par with international mainstream methods |
4. Implementation Suggestions
Laboratory Preparation:Equipped with GC/MS equipment, ultrasonic generator, vertical oscillator and other instruments to ensure that reagents and materials meet the analytical purity requirements.
Sample Processing:It is recommended to take samples according to the standard regulations and pay attention to the representativeness of the samples. For complex samples, crushing and mixing can be performed in advance.
Data Recording:Detailed records of the test conditions, results and deviation analysis of each batch of samples are required to facilitate subsequent traceability and improvement.

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