GB/T 35828-2018 in English

VALID

Determination of chromium,arsenic,cadmium,stibium,and lead in cosmetics—Inductively coupled plasma mass spectrometry

Issued on:2018-02-06
Implemented on:2018-09-01
File Format:PDF
Delivery:Via email within 1~3 business days

Price(USD)： $130.00
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Standard No:	GB/T 35828-2018
Document status:	VALID
Title in English:	Determination of chromium,arsenic,cadmium,stibium,and lead in cosmetics—Inductively coupled plasma mass spectrometry
Title in Chinese:	化妆品中铬、砷、镉、锑、铅的测定电感耦合等离子体质谱法
Language:	English
File Format:	Electronic (PDF)
Delivery:	Via email within 1~3 business days
Issued on:	2018-02-06
Implemented on:	2018-09-01
ICS Classification:	71.100.70-Cosmetics. Toiletries
Chinese Classification:	Y42-Cosmetics
Professional Classification:	GB-National Standard
Related Keywords:	plasma mass spectrometry plasma mass spectrometry introduction gb/t mass spectrometry separation icp-ms arsenic icp-ms cadmium
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《GB/T 35828-2018化妆品中铬、砷、镉、锑、铅的测定电感耦合等离子体质谱法》由TC257（全国香料香精化妆品标准化技术委员会）归口，TC257SC2（全国香料香精化妆品标准化技术委员会化妆品分会）执行，主管部门为中国轻工业联合会。

Introduction

GB/T 35828—2018 Standard Overview

GB/T 35828—2018 "Determination of chromium, arsenic, cadmium, antimony and lead in cosmetics by inductively coupled plasma mass spectrometry" is one of the core standards in the field of cosmetics testing in my country. This standard specifies the method of determining chromium, arsenic, cadmium, antimony and lead in cosmetics by inductively coupled plasma mass spectrometry (ICP-MS), which is applicable to a variety of cosmetic products such as face creams, lotions, lip glosses, etc.

Background and significance of standard formulation

This standard is formulated based on the requirements of the "Technical Specification for Safety of Cosmetics (2015 Edition)" and clarifies the detection methods for the prohibited substances chromium, arsenic, cadmium, antimony and lead. These substances are listed as prohibited raw materials because they may cause serious harm to human health. Although my country has not yet stipulated the limit values of chromium and antimony, this standard provides a scientific basis for the detection of these elements in cosmetics.

Technical framework and core content

The core content of this standard includes:

Principle and application of inductively coupled plasma mass spectrometry (ICP-MS)
Requirements for reagents and materials
Technical parameters of instruments and equipment
Sample preparation and digestion methods
Preparation of standard series
Calculation and analysis of measurement results

Core technical indicator comparison table

Element	Detection limit (mg/kg)	Quantification limit (mg/kg)	Analysis method
Element	Detection limit (mg/kg)	Quantification limit (mg/kg)	Analysis method
Chromium (Cr)	0.07	0.2	ICP-MS
Arsenic (As)	0.07	0.2	ICP-MS
Cadmium (Cd)	0.04	0.1	ICP-MS
Antimony (Sb)	0.07	0.2	ICP-MS
Lead (Pb)	0.07	0.2	ICP-MS

Instrument Principle and Process

The working principle of inductively coupled plasma mass spectrometry (ICP-MS) involves the following key steps:

Sample digestion: completed by microwave digestion or graphite digestion system to ensure that the elements to be measured are completely released.

Atomization and ionization: The sample solution enters the plasma torch flame through the atomizer to form positively charged ions.

Mass spectrometry separation: Ions are separated and detected according to the mass-to-charge ratio (m/z), and the signal intensity is proportional to the element concentration.

Data processing: Quantitative analysis is achieved through the standard curve method, and the matrix interference is eliminated in combination with the internal standard method.

Implementation suggestions and precautions

To ensure the accuracy and reliability of the test results, it is recommended in actual operation:

Select reagents and instruments in strict accordance with standard requirements.

Standardize the sample preparation process to avoid external contamination.

Regularly calibrate the instrument to ensure that the sensitivity and precision meet the requirements.

Establish a quality control system, including blank tests, parallel sample analysis, etc.

More samples: NB/T 47013.2-2015 YD/T 3934-2021 DL/T 368-2010

Sample only — not a preview of GB/T 35828-2018

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