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polycyclic aromatic hydrocarbons gas chromatography-mass spectrometry introduction gb/t leather chemical tests determination leather chemical tests gas chromatography-mass spectrometry polycyclic aromatic hydrocarbons safety factors optical crystals hose assemblies textile-reinforced types
GB/T 36946-2018 in English

GB/T 36946-2018 in English

VALID

Leather—Chemical tests—Determination of polycyclic aromatic hydrocarbons—Gas chromatography-mass spectrometry

  • Issued on:2018-12-28
  • Implemented on:2019-07-01
  • File Format:PDF
  • Delivery:Within 1 day
Price(USD): $128.00
$125.00
Standard No: GB/T 36946-2018
Document status: VALID
Title in English: Leather—Chemical tests—Determination of polycyclic aromatic hydrocarbons—Gas chromatography-mass spectrometry
Title in Chinese: 皮革 化学试验 多环芳烃的测定 气相色谱-质谱法
Language: English
File Format: Electronic (PDF)
Delivery: Within 1 day
Issued on: 2018-12-28
Implemented on: 2019-07-01
ICS Classification: 59.140.30-Leather and furs
Chinese Classification: Y46-Furs and leathers
Professional Classification: GB-National Standard
Related Keywords: polycyclic aromatic hydrocarbons gas chromatography-mass spectrometry introduction gb/t
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gb/t 36946

《GB/T 36946-2018皮革 化学试验 多环芳烃的测定 气相色谱-质谱法》由TC252(全国皮革工业标准化技术委员会)归口,主管部门为中国轻工业联合会。


Introduction

GB/T 36946-2018 Standard Overview

GB/T 36946-2018 is a national standard of the People's Republic of China, entitled Leather Chemical Tests - Determination of Polycyclic Aromatic Hydrocarbons - Gas Chromatography-Mass Spectrometry. This standard specifies the specific method for the detection of 16 polycyclic aromatic hydrocarbons (PAHs) in leather and leather products using gas chromatography-mass spectrometry (GC/MS).

Background of Standard Formulation

PAHs are a class of highly toxic and carcinogenic chemicals that are widely present in industrial pollutants and the environment. During the leather manufacturing process, these harmful substances may remain in the finished product, posing a threat to human health and the environment. Therefore, establishing an effective detection method is crucial to ensure product quality and consumer safety.

Technology Evolution Analysis

The detection of PAHs has evolved from traditional spectrophotometry to modern chromatography technology. Gas chromatography-mass spectrometry has become one of the most commonly used detection methods due to its high sensitivity, efficiency and accuracy. This standard adopts the advanced GC/MS method and combines it with the selected ion monitoring mode (SIM), which significantly improves the detection efficiency and accuracy.

Comparison of standard frameworks

Standard dimensions GB/T 36946-2018 Reference GB/T28189—2011
Detection method GC/MS, selected ion monitoring mode GCC, flame ionization detector
Scope of application 16 PAHs in leather and products PAHs in textiles
Sensitivity Lower detection limit: 2.0-1.0 mg/kg Lower detection limit: Unspecified

Implementation recommendations

Precautions for experimental operation

  • Sample handling:Ensure that the sampling site complies with the provisions of QB/T 2706 to avoid contamination.
  • Extraction and purification:When using ultrasonic extraction and silica gel solid phase extraction column purification, pay attention to controlling the flow rate and eluent ratio.
  • Instrument calibration:Regularly calibrate the GC/MS system to ensure the stability of the chromatographic column and ion source temperature.

Data analysis and quality control

  • Blank test:Perform at least one blank test for each batch of samples to ensure data reliability.
  • Recovery verification:The recovery rate of the standard working solution should not be less than 80% to ensure the accuracy of the method.
  • Result Report: Record sampling information, abnormal phenomena and operation steps that do not meet the standards in detail.

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