GB/T 39107-2020 in English
VALIDDetermination of volatile organic compounds content for consumer products—Static headspace sampling method
- Issued on:2020-10-21
- Implemented on:2020-10-21
- File Format:PDF
- Delivery:Via email within 1~3 business days
$194.00
《GB/T 39107-2020消费品中可挥发性有机物含量的测定 静态顶空进样法》由TC508(全国消费品安全标准化技术委员会)归口,主管部门为国家标准化管理委员会。
Introduction
Analysis of the core content of the standard
| Test substances | Detection limit (mg/kg) | Quantification limit (mg/kg) | Retention time (min) |
|---|---|---|---|
| Dichloromethane | 1.0 | 2.0 | 8.94(GC-MS)/10.30(GC-FID) |
| Benzene | 1.0 | 2.0 | 13.35(GC-MS)/14.09(GC-FID) |
Key technical requirements
Instrument configuration:It needs to be equipped with static headspace sampler, gas chromatograph (with FID detector or MS detector), headspace bottle volume 20mL, sample volume 0.02g±0.002g.
Method validation:The spike recovery rate needs to be controlled between 80.4%-118.4%, and the relative standard deviation (RSD) ≤20%.
Implementation recommendations
- Pay attention to sealing during sample pretreatment to prevent VOCs from volatilizing
- It is recommended to use the internal standard method (toluene-d8) for quantitative analysis
- For co-eluting components such as o-/p-xylene, it is necessary to distinguish them by mass spectrometry characteristic ions
Background of standard evolution
This standard replaces the original industry method. The main improvements include: ①Adding new VOCs detection indicators such as isophorone; ②Optimizing the heating program (initial 40℃ for 2min, final 230℃); ③Clarifying the mass spectrometry parameters of the SIM scanning mode.

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