GB/T 43861-2024 in English

VALID

General rules for microwave plasma atomic emission spectrometry

Issued on:2024-04-25
Implemented on:2024-04-25
File Format:PDF
Delivery:Via email within 5 business days

Price(USD)： $310.00
$301.00

Standard No:	GB/T 43861-2024
Document status:	VALID
Title in English:	General rules for microwave plasma atomic emission spectrometry
Title in Chinese:	微波等离子体原子发射光谱方法通则
Language:	English
File Format:	Electronic (PDF)
Delivery:	Via email within 5 business days
Issued on:	2024-04-25
Implemented on:	2024-04-25
Professional Classification:	GB-National Standard
Related Keywords:	microwave plasma atomic emission spectrometry plasma atomic emission spectrometry introduction atomic emission spectrometry microwave plasma method microwave plasma
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《GB/T 43861-2024微波等离子体原子发射光谱方法通则》由TC481（全国仪器分析测试标准化技术委员会）归口，主管部门为科技部。

Introduction

1. Standard Overview

GB/T 43861-2024 "General Rules for Microwave Plasma Atomic Emission Spectrometry" is my country's first general standard for microwave plasma atomic emission spectroscopy (MIP-AES) technology. This standard clarifies the application specifications of MIP-AES in the qualitative and quantitative analysis of metals and some non-metallic elements, and is applicable to sample detection under liquid injection mode.

2. Comparison of the core of the standard framework

Standard dimensions	GB/T 43861—2024	ICP-AES comparison	Flame AAS comparison
Sensitivity	ppb level	Better than traditional flame method, up to ppq level	Poor
Detection limit	Metal elements: 1 ng/mL; non-metal elements: 5 ng/mL	Metal elements: 0.5 ng/mL	Metal elements: 5 ng/mL
Matrix effect processing capability	Good, supports multiple correction methods	Good	Poor

3. Principle and scope of application of the method

Microwave plasma atomic emission spectrometry (MIP-AES) is a technology that uses plasma excited by microwave energy as a light source to achieve qualitative and quantitative detection by analyzing the wavelength and intensity of characteristic radiation of elements in the sample.

Application case: Heavy metal detection in environmental monitoring

MIP-AES can be used to determine heavy metals such as cadmium and lead in water samples. By preparing a standard solution with a concentration gradient and using the standard curve method for quantitative analysis, the detection limit can reach 0.1 ng/mL.

4. Implementation Suggestions

Instrument selection and configuration:Prioritize the use of a high-sensitivity microwave plasma mass spectrometer to ensure the stability of the gas path system and the uniformity of the light source.
Sample pretreatment:For solid samples, it is recommended to use wet digestion combined with microwave-assisted oxidation technology; liquid samples can be directly injected or measured after dilution.
Interference elimination:Effectively reduce physical and ionization interferences by optimizing instrument parameters (such as carrier gas flow rate, power), matrix matching and internal standard method.
Quality control:Regularly use certified reference materials for calibration, and establish a complete quality control process, including blank tests, spike recovery tests, etc.

More samples: JJG 21-2008 YD/T 3934-2021 GB 50021-2001(2009)

Sample only — not a preview of GB/T 43861-2024

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