GBZ/T 300.130-2017 in English
VALIDDetermination of toxic substances in workplace air―Part 130: Dibutyl phthalate and diotyl phthalate
- Issued on:2017-11-09
- Implemented on:2018-05-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$117.00
GBZ/T 300的本部分规定了工作场所空气中邻苯二甲酸二丁酯和邻苯二甲酸二辛酯的溶剂解吸-高效液相色谱法和邻苯二甲酸二丁酯的溶剂洗脱-气相色谱法。
本部分适用于工作场所空气中邻苯二甲酸二丁酯和邻苯二甲酸二辛酯浓度的检测。
Introduction
1. Scope of the standard and normative references
This standard applies to the detection of dibutyl phthalate and dioctyl phthalate concentrations in workplace air, and specifies two detection methods: solvent desorption-high performance liquid chromatography and solvent elution-gas chromatography.
3. Solvent desorption-High Performance Liquid Chromatography (HPLC)
Principle: Vapor-state phthalates in the air are collected by silica gel, desorbed by methanol and injected, separated by a C18 liquid chromatography column and detected by a UV detector.
Method Comparison Analysis
| Project | HPLC method | GCF method |
|---|---|---|
| Detection sensitivity | Detection limit: 0.07μg/mL | Detection limit: 12μg/mL |
| Applicable scenarios | Vapor state detection | Aerosol state detection |
4. Solvent elution-gas chromatography (GC)
Principle: Aerosol-state dibutyl phthalate in the air is collected with a microporous filter, eluted with carbon disulfide, separated by a gas chromatography column, and detected by a hydrogen flame ionization detector.
5. Implementation suggestions
- Choose an appropriate method (HPLC or GC) according to the specific conditions of the workplace.
- Calibrate the equipment regularly to ensure that the instrument is in the best condition.
- Strengthen personnel training to improve operational standardization and data analysis capabilities.
- Establish a quality control system to ensure the accuracy and reliability of test results.

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