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dibutyl phthalate aerosol-state dibutyl phthalate diotyl phthalate introduction dioctyl phthalate workplace air ― part non-fried instant noodles movable bar chairs radar equipment
GBZ/T 300.130-2017 in English

GBZ/T 300.130-2017 in English

VALID

Determination of toxic substances in workplace air―Part 130: Dibutyl phthalate and diotyl phthalate

  • Issued on:2017-11-09
  • Implemented on:2018-05-01
  • File Format:PDF
  • Delivery:Via email within 1~3 business days
Price(USD): $120.00
$117.00
Standard No: GBZ/T 300.130-2017
Document status: VALID
Title in English: Determination of toxic substances in workplace air―Part 130: Dibutyl phthalate and diotyl phthalate
Title in Chinese: 工作场所空气有毒物质测定 第130部分:邻苯二甲酸二丁酯和邻苯二甲酸二辛酯
Language: English
File Format: Electronic (PDF)
Delivery: Via email within 1~3 business days
Issued on: 2017-11-09
Implemented on: 2018-05-01
Superseding: GBZ/T 160.66-2004 Methods for determination of aromatic esters in the air of workplace
ICS Classification: 13.100-Occupational safety. Industrial hygiene
Chinese Classification: C52-Labor sanitation
Professional Classification: GBZ-Professional Health
Related Keywords: dibutyl phthalate
aerosol-state dibutyl phthalate
diotyl phthalate introduction
dioctyl phthalate
workplace air ― part
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GBZ/T 300的本部分规定了工作场所空气中邻苯二甲酸二丁酯和邻苯二甲酸二辛酯的溶剂解吸-高效液相色谱法和邻苯二甲酸二丁酯的溶剂洗脱-气相色谱法。
本部分适用于工作场所空气中邻苯二甲酸二丁酯和邻苯二甲酸二辛酯浓度的检测。


Introduction

1. Scope of the standard and normative references

This standard applies to the detection of dibutyl phthalate and dioctyl phthalate concentrations in workplace air, and specifies two detection methods: solvent desorption-high performance liquid chromatography and solvent elution-gas chromatography. C24H38O4 390.56 Dibutyl phthalate 84-74-2 C16H22O4 278.34 Dioctyl phthalate 117-81-7 C24H38O4 390.56

3. Solvent desorption-High Performance Liquid Chromatography (HPLC)

Principle: Vapor-state phthalates in the air are collected by silica gel, desorbed by methanol and injected, separated by a C18 liquid chromatography column and detected by a UV detector.

Method Comparison Analysis

Project HPLC method GCF method
Detection sensitivity Detection limit: 0.07μg/mL Detection limit: 12μg/mL
Applicable scenarios Vapor state detection Aerosol state detection

4. Solvent elution-gas chromatography (GC)

Principle: Aerosol-state dibutyl phthalate in the air is collected with a microporous filter, eluted with carbon disulfide, separated by a gas chromatography column, and detected by a hydrogen flame ionization detector.

5. Implementation suggestions

  • Choose an appropriate method (HPLC or GC) according to the specific conditions of the workplace.
  • Calibrate the equipment regularly to ensure that the instrument is in the best condition.
  • Strengthen personnel training to improve operational standardization and data analysis capabilities.
  • Establish a quality control system to ensure the accuracy and reliability of test results.

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