SN/T 5233-2020 in English
VALIDImport and export textile material Test of moisture regain of raw cotton-Near infrared spectroscopy method
- Issued on:2020-08-27
- Implemented on:2021-03-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$185.00
Introduction
Analysis of the core content of the standard
This standard for the first time incorporates Fourier transform near-infrared spectrometer and grating scanning fiber spectrometer into the raw cotton regain detection system, and specifies the technical parameter requirements of the two instruments:
| Instrument type | Wavelength range | Resolution | Signal-to-noise ratio | Modeling method |
|---|---|---|---|---|
| Fourier transform type | 4000-10000 cm⁻¹ | 8 cm⁻¹ | 10000:1 | Partial least squares method |
| Raster scanning type | 1000-1800 nm | 10 nm | 30000:1 | Partial least squares method |
Technical principles and innovations
Rapid detection is achieved by establishing a mathematical model of the raw cotton spectrum and the values measured by the oven method, utilizing the combined frequency absorption band characteristics of water molecules in the near-infrared region. Key technological breakthroughs include:
- Savitzky-Gloay smoothing and first-order derivative preprocessing are used to eliminate background interference
- Model transfer technology ensures consistency of results between different instruments (absolute error ≤ 0.5%)
- Three-dimensional sampling design (front/back/inner layer) reduces the impact of fiber unevenness
Key points of operating specifications
Typical application cases
In a customs laboratory's test of batches of U.S. cotton, the near-infrared method measured a regain of 8.2%±0.3%, which was consistent with the result of 8.0% by the oven method. The testing time for a single sample was shortened from 4 hours to 5 minutes.
Abnormal handling process
When the difference between two measurements is >0.5% or the result is outside the range of 6-15%, you need to:
- Check whether the sample contains weeds/foreign fibers
- Resample and test
- If still abnormal, switch to the GB/T 6102.1 oven method
Implementation suggestions
Laboratories should pay attention to the following when introducing this standard:
- Instrument verification:Must pass the accuracy (SEP≤1.0%) and repeatability (≤0.5%) verification in Appendix A
- Model maintenance:Use monitoring samples for daily calibration, and remodeling is required if the deviation exceeds the limit
- Staff training:Focus on mastering the spectral acquisition specifications (sampling bottle pressure, rotation speed, etc.)

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