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SN/T 5233-2020 in English

SN/T 5233-2020 in English

VALID

Import and export textile material Test of moisture regain of raw cotton-Near infrared spectroscopy method

  • Issued on:2020-08-27
  • Implemented on:2021-03-01
  • File Format:PDF
  • Delivery:Via email within 1~3 business days
Price(USD): $190.00
$185.00
Standard No: SN/T 5233-2020
Document status: VALID
Title in English: Import and export textile material Test of moisture regain of raw cotton-Near infrared spectroscopy method
Title in Chinese: 进出口纺织原料 原棉回潮率测定 近红外光谱法
Language: English
File Format: Electronic (PDF)
Delivery: Via email within 1~3 business days
Issued on: 2020-08-27
Implemented on: 2021-03-01
Professional Classification: SN-Import&Export Inspection
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Introduction

Analysis of the core content of the standard

This standard for the first time incorporates Fourier transform near-infrared spectrometer and grating scanning fiber spectrometer into the raw cotton regain detection system, and specifies the technical parameter requirements of the two instruments:

Instrument type Wavelength range Resolution Signal-to-noise ratio Modeling method
Fourier transform type 4000-10000 cm⁻¹ 8 cm⁻¹ 10000:1 Partial least squares method
Raster scanning type 1000-1800 nm 10 nm 30000:1 Partial least squares method

Technical principles and innovations

Rapid detection is achieved by establishing a mathematical model of the raw cotton spectrum and the values measured by the oven method, utilizing the combined frequency absorption band characteristics of water molecules in the near-infrared region. Key technological breakthroughs include:

  1. Savitzky-Gloay smoothing and first-order derivative preprocessing are used to eliminate background interference
  2. Model transfer technology ensures consistency of results between different instruments (absolute error ≤ 0.5%)
  3. Three-dimensional sampling design (front/back/inner layer) reduces the impact of fiber unevenness

Key points of operating specifications

Typical application cases

In a customs laboratory's test of batches of U.S. cotton, the near-infrared method measured a regain of 8.2%±0.3%, which was consistent with the result of 8.0% by the oven method. The testing time for a single sample was shortened from 4 hours to 5 minutes.

Abnormal handling process

When the difference between two measurements is >0.5% or the result is outside the range of 6-15%, you need to:

  1. Check whether the sample contains weeds/foreign fibers
  2. Resample and test
  3. If still abnormal, switch to the GB/T 6102.1 oven method

Implementation suggestions

Laboratories should pay attention to the following when introducing this standard:

  • Instrument verification:Must pass the accuracy (SEP≤1.0%) and repeatability (≤0.5%) verification in Appendix A
  • Model maintenance:Use monitoring samples for daily calibration, and remodeling is required if the deviation exceeds the limit
  • Staff training:Focus on mastering the spectral acquisition specifications (sampling bottle pressure, rotation speed, etc.)

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