SY/T 5121-2021 in English
VALIDMethods for infrared spectrometric analysis of organic matter and crude oil in rocks
- Issued on:2021-11-16
- Implemented on:-
- File Format:PDF
- Delivery:Via email within 1~3 business days
$204.00
Introduction
Analysis of the evolution of standard technology
| Version | Main improvements | Technical significance |
|---|---|---|
| SY/T 5121-1986 | Basic method framework | Establish the application foundation of infrared spectroscopy in the field of oil and gas geology |
| SY/T 5121-2021 | Add microscopic infrared and ATR methods, and improve the parameter system | Realize micro-area analysis and rapid detection of complex samples |
Core instrument configuration requirements
Key equipment technical indicators:
- Fourier transform infrared spectrometer: wave number range 4000-400cm⁻¹, resolution ≥4cm⁻¹
- Infrared microscope: magnification ≥320× (MCT low temperature detector required)
- ATR accessory: suitable for non-destructive testing of liquid samples
Critical control points of sample preparation
| Sample type | Preparation method | Quality requirements |
|---|---|---|
| Kerogen | KBr tablet method (particle size <10μm) | Transmittance 20-80% |
| Crude oil components | Smear method (zinc selenide wafer) | Film thickness is uniform and has no interference fringes |
| Hydrocarbon inclusions | Microscopic infrared thin section method | Thickness ≤3μm |
Organic matter maturity evaluation system
Core calculation parameters:
- Aliphatic chain parameters (CH2/CH3): Reflects the degree of thermal evolution of organic matter
- Aromatization index (1600cm⁻¹/1460cm⁻¹): Characterizes the aromatization process
- Z factor (720cm⁻¹/750cm⁻¹): Distinguishes the source of parent materials
Typical application case: The maturity evaluation of Gulong shale in Daqing Oilfield shows that the CH2/CH3 ratio drops from 0.8 (low maturity) to 0.3 (high maturity)
Implementation suggestions
Laboratory operation precautions:
- Strictly control humidity <60% to avoid the influence of KBr moisture absorption
- Background subtraction (blank wafer) is required before microscopic infrared analysis
- Regularly calibrate the instrument wavenumber accuracy with polystyrene standard sheets

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