YS/T 1563.4-2022 in English

VALID

Methods for chemical analysis of molybdenum rhenium alloy- Part 4: Determination of aluminum, calcium, copper, iron, magnesium, manganese, nickel, tin and tungsten contents- Inductively coupled plasma mass spectrometry

Issued on:2022-09-30
Implemented on:2023-04-01
File Format:PDF
Delivery:Via email within 1~3 business days

Price(USD)： $270.00
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Standard No:	YS/T 1563.4-2022
Document status:	VALID
Title in English:	Methods for chemical analysis of molybdenum rhenium alloy- Part 4: Determination of aluminum, calcium, copper, iron, magnesium, manganese, nickel, tin and tungsten contents- Inductively coupled plasma mass spectrometry
Title in Chinese:	钼铼合金化学分析方法第4部分：铝、钙、铜、铁、镁、锰、镍、锡、钨含量的测定电感耦合等离子体质谱法
Language:	English
File Format:	Electronic (PDF)
Delivery:	Via email within 1~3 business days
Issued on:	2022-09-30
Implemented on:	2023-04-01
Professional Classification:	YS-Non-ferrous Metal
Related Keywords:	plasma mass spectrometry introduction interpretation standard technology analysis dimension features plasma mass spectrometer traditional methods detection chemical analysis
Related Topics:	inductive coupling inductive coupling Rhenium Ionization Mass Spectrometry Inductively Coupled Plasma Mass Spectrometry Coupled inductor aluminum calcium aluminum calcium plasma mass spectrometry ys/t 4 plasma mass spectrometry Tungsten tin Coupled inductor Inductively Coupled Plasma Measurements Inductively Coupled Plasma Mass Spectrometry Separation of molybdenum and aluminum Ionization Methods for Mass Spectrometry Iron Manganese Nickel Chemical Analysis Method of Al-Mn-Fe Alloy Coupled Inductance Measurement Determination of Tungsten Content in Iron and Steel by Inductive Coupling molybdenum iron inductive coupling YS/T 1562.3-2022 Copper-nickel separation method Method for masking metal cations iron, magnesium and aluminum Chemical analysis method of molybdenum-rhenium alloy ys/t 1523-2022 ys/t1568-2022

本文件规定了钼铼合金中铝、钙、铜、铁、镁、锰、镍、锡、钨含量的测定方法。
本文件适用于钼铼合金中铝、钙、铜、铁、镁、锰、镍、锡、钨含量的测定。各元素的测定范围：0.0001%～0.010%。

Introduction

Interpretation of standard technology

Analysis dimension	Features of YS/T 1563.4	Comparison with traditional methods
Detection limit	Ultra-low detection limit of 0.1μg/g	Conventional AAS is 1-10μg/g
Multi-element synchronization	Simultaneous determination of 9 elements	Multiple experiments are required
Hydrofluoric acid resistant system	Equipped with a dedicated sample injection system	Ordinary ICP-MS is prone to corrosion

Core Technology Innovation

The standard adopts inductively coupled plasma mass spectrometer combined with collision reaction cell technology, and optimizes the detection conditions for easily interfered elements such as Ca and Fe. Sc(45) and Cs(133) are selected as internal standard elements to correct the signal drift of light and heavy elements respectively.

Implementation Points

Typical Application Case: The detection of a certain aviation-grade molybdenum-rhenium alloy sample showed that the Mn content was 0.0023%, and the RSD of repeated determination was only 2.1%, which fully met the repeatability limit of 0.0003% required by the standard.

Background of Standard Evolution

With the expansion of the application of molybdenum-rhenium alloy in key components such as aerospace engine nozzles, this part has been added to the original YS/T standard system to fill the gap in the detection method of ultra-trace impurities. Compared with the 2005 series of standards, the 2022 version has a 10-100 times higher detection sensitivity.

More samples: NB/T 47013.2-2015 JJG 21-2008 QC/T 942-2021

Sample only — not a preview of YS/T 1563.4-2022

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