GB/T 13241-2017 in English
VALIDIron ores--Determination of reducibility
- Issued on:2017-09-07
- Implemented on:2018-06-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$175.00
《GB/T 13241-2017铁矿石 还原性的测定方法》由TC317(全国铁矿石与直接还原铁标准化技术委员会)归口,主管部门为中国钢铁工业协会。
Introduction
Interpretation of GB/T 13241—2017 National Standard of the People's Republic of China
Standard Background and Revision Notes
GB/T 13241—2017 "Determination of the Reducibility of Iron Ore" was issued in 2017, replacing the old version of the standard in 1991. This revision mainly improves the following aspects:
- Modified normative references
- Clarified the requirements for mass flow controllers of test equipment
- Improved gas control accuracy
- Added an appendix description of CO generator
Core Principles of Determination of Reducibility of Iron Ore
This standard adopts the fixed bed method and uses a mixed gas of CO and N2 (30% CO ±0.5%, 70% N2 ±0.5%) for isothermal reduction at 900°C. By measuring the mass loss of an iron ore sample over a certain period of time, its reduction degree and reduction rate index are calculated.
Key term explanation and practical application cases
| Terms | Definition | Application scenario |
|---|---|---|
| Reduction degree (Rt) | The degree of deoxidation achieved after a certain period of reduction based on the trivalent iron state. | Used to evaluate the performance of iron ore in the blast furnace ironmaking process. |
| Reduction rate index (RVI) | The degree of reduction per unit time when the atomic ratio O/Fe is 0.9. | Used to predict the reaction rate of iron ore during the smelting process. |
Comparative Analysis of Standard Frameworks
The following is a comparison of the main technical differences between GB/T 13241—2017 and GB/T 13241—1991:
| Standard Dimensions | GB/T 13241—1991 | GB/T 13241—2017 |
|---|---|---|
| Gas Composition Requirements | The ratio and purity of CO and N2 are not specified | 30% CO ±0.5%, 70% N2 are specified ±0.5%, and gas purity ≥99.9% |
| Flow control accuracy | The flow controller accuracy requirement is not specified | The flow controller accuracy is specified to be no less than ±1.5% FS |
| Temperature control range | The temperature control accuracy is not specified | 900°C ±5°C is clearly required, and the temperature control accuracy is not less than Class 0.2 |
Implementation suggestions and precautions
Key equipment selection: When selecting a mass flow controller, ensure that its range and accuracy meet the standard requirements (CO: 5 L/min, N2: 20 L/min, accuracy ±1.5% FS). It is recommended to calibrate the flowmeter and thermocouple at least once a year.
Experimental environment safety:Since the test involves toxic gas (CO), the test site must be well ventilated and equipped with a CO alarm. Operators should wear protective equipment and regularly test the CO concentration in the environment to ensure that it does not exceed 50×10-6.
Data recording and processing:It is recommended to use a thermogravimetric balance to continuously record the change in sample mass and perform numerical rounding according to GB/T 8170. For the calculation of the reduction index RI and the reduction rate index RVI, it is necessary to strictly follow the standard formula to ensure that the results are accurate to one decimal place.
Summary
GB/T 13241-2017 "Determination of the reducibility of iron ore" significantly improves the accuracy of the determination of the reducibility of iron ore by introducing stricter gas control, temperature control accuracy and equipment calibration requirements. This standard provides a scientific and technical basis for the metallurgical industry, helps optimize the ironmaking process and improve product quality.

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