GB/T 17280-2017 in English

VALID

Standard test method for distillation of crude petroleum―15-theoretical plate column

Issued on:2017-12-29
Implemented on:2018-07-01
File Format:PDF
Delivery:Via email within 5 business days

Price(USD)： $690.00
$670.00

Standard No:	GB/T 17280-2017
Document status:	VALID
Title in English:	Standard test method for distillation of crude petroleum―15-theoretical plate column
Title in Chinese:	原油蒸馏标准试验方法 15-理论塔板蒸馏柱
Language:	English
File Format:	Electronic (PDF)
Delivery:	Via email within 5 business days
Issued on:	2017-12-29
Implemented on:	2018-07-01
Superseding:	GB/T 17280-2009 Standard test method for distillation of crude petroleum - 15-theoretical plate column
ICS Classification:	75.040-Crude petroleum
Chinese Classification:	E21-Crude petroleum
Professional Classification:	GB-National Standard
Related Keywords:	parameters distillation pressure segmentation standard test method technical parameters conformity verification method distillation column inner diameter specifications validation cycle distillation column appendix f dynamic response test key
Related Topics:	tower principle Total cyanide distillation method Distillation value distilled aluminum Solid Distillation Apparatus Distillation tester Rotary distillation Column principle Rotary evaporator distiller How to use the distiller Sample still Column instrument principle Petroleum distillation machine Petroleum distillation machine Principle of steam instrument t3 column principle distillate standard oil Petroleum Distiller Petroleum Distiller automatic still standard still use t3 column principle Rotary distillation and distillation crude oil evaporation distilled six eight Distillation tester Distillation experiment Steam Distillation experiment Laboratory Distillation Method Distillation distillation apparatus Range distillation to distill Distillation principle carry out distillation isothermal distillation total cyanide distillation Distillation and Extraction Diesel Distiller steam distillation indirect method theoretical board Petroleum Distillation Equipment plate theory distillate+ Principle of standard method The principle of fractionation distillation foam Distillation commissioning theoretical plate Distiller UV UV distiller Petroleum Fraction Distillation board principle distilled recently isothermal distillation semi-theoretical approach Methods of Industrial Distillation Distillation reverse still section why when distilled Evaporators and Distillers crude oil vapor distillation test astm eight stage distillation solid distillation Distillers and Evaporators theoretical plate Methods of Industrial Distillation Pre-column principle total cyanide distillation distillation ball distillation and evaporation Distillation and Evaporation industrial distillation Distillation range of crude oil distillation Petroleum Distillation Equipment Evaporators and Distillers distilled and evaporated Test Theory and Methods parametric distillation test theory method distilled iodometric method second-hand petroleum distiller still method Distillation test method oxidative distillation Distillation method of distillation Distilled food Automatic Distillation Tester distilled strontium two distillation methods double still How to Distill Acid Method of Distillation Unit Distillation/Evaporation GBT17280 GBT17280-1998 GB/T 17280-2009 GB/T 17280-2017 number of theoretical plates Advantages of distillation Distilled tin Low number of theoretical plates Distillation instrument AD-6 Ephedra water distillation method The latest national standards for distilled water Principle of internal standard standard curve method How to increase the number of theoretical plates Crude oil fraction division Calibrate your own distillation Reasons why the national standard distillation method for measuring moisture is inaccurate Distilled water quality standards (national standard) Are there standards for distilled water? Distillation method of pure water National standards for distilled water inspection Principle of Chinese Fayan separation method distillation principle Distillation air tightness inspection method Crude oil distillation range determination method Ammonia steam tower industry Number of theoretical plates for method validation Is there a national standard for distillers? Is there an industry standard for distilled water? Distilled water standard indicators What are the methods of distillation? Principle of standard addition method Principles of column chromatography Standard method for true boiling point distillation Detection Method of Petroleum Toluene Distillation gb17280 gb/t 17280 Theoretical plate number calculation method

《GB/T 17280-2017原油蒸馏标准试验方法 15-理论塔板蒸馏柱》由TC355（全国石油天然气标准化技术委员会）归口，TC355SC10（全国石油天然气标准化技术委员会油气计量及分析方法分会）执行，主管部门为国家标准化管理委员会。

Introduction

Analysis of the core content of the standard

Main updates: New nitrogen purge specifications (Appendix E), quality assurance chapter (Chapter 13) and pressure gauge calibration requirements (5.3.2)

Instrument system composition

Components	Key technical parameters	Conformity verification method
Distillation column	Inner diameter 25-70mm, 14-18 theoretical plates	Appendix B n-heptane-methylcyclohexane test
Reflux distributor	Separation accuracy ≥ 90%, cycle 18-30s	Appendix D Reflux ratio verification
Temperature sensor	Response time ≤ 175s, accuracy 0.5℃	Appendix F Dynamic response test

Key operating parameters

Distillation pressure segmentation:

Atmospheric pressure (101.3kPa)
Medium pressure (13.3kPa)
Low pressure (1.33-0.266kPa)

Reflux ratio control:

Normal pressure section 5:1
0.674-0.27kPa pressure section 2:1

Typical operation case

For Propak packed column, at a reflux ratio of 5:1, the evaporation rate should be controlled at 75% of 670mL/(h·cm²) (about 500mL/(h·cm²)), and the pressure drop should be maintained within 0.84kPa/m.

Technology Evolution Analysis

Main Improvements from 2009 Edition to 2017 Edition

Safety Enhancement: Added specifications for dehydration of water-containing crude oil (Appendix J) and hydrogen sulfide protection warnings
Data Reliability: New Chapter 13 Quality Assurance System, requiring the establishment of a quality control sample analysis mechanism
Instrument Compatibility: Allows the use of equivalent vacuum gauges/pressure gauges to replace the original standard devices

Implementation Recommendations

Laboratory Configuration Plan

Equipment Type	Recommended Specifications	Validation Cycle
Distillation Column	50mm inner diameter, 6mm Propak packing	Annual inspection (Appendix I)
Temperature sensor	Platinum resistance, response time ≤150s	Monthly calibration (Appendix G)

Common problem handling

Flooding:Immediately reduce the heating power and the cut fraction needs to be returned to the kettle for re-distillation
Yield loss>0.4%:2/3 allocated to the cold trap fraction and 1/3 included in the first fraction

More samples: JJG 21-2008 YD/T 3934-2021 JC/T 2453-2018

Sample only — not a preview of GB/T 17280-2017

Loading PDF document...

Error loading PDF. Please make sure the file is valid and try again.

We also recommend

GB/T 17282-2012 in English

Test method for estimation of mean relative molecular mass of petroleum oils from viscosity measurements
2012-12-31
GB/T 6531-1986 in English

Crude petroleum and fuel oils; Determination of sediment; Extraction method
1986-06-25
GB/T 25104-2019 in English

Automatic measurement of water content in crude oil—RF method
2019-08-30
GB/T 17606-2009 in English

Determination of sulfur in crude-oil by energy-dispersive X-ray fluorescence spectrometry
2009-04-08
GB/T 26982-2022 in English

Determination of wax content in crude oil
2022-03-09