GB/T 23669-2016 in English
VALID2,6-Dibromo-4-nitroaniline
- Issued on:2016-12-30
- Implemented on:2017-07-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$156.00
《GB/T 23669-20162,6-二溴-4-硝基苯胺》由TC134(全国染料标准化技术委员会)归口,主管部门为中国石油和化学工业联合会。
Introduction
Overview of GB/T 23669-2016 Standard
GB/T 23669-2016 "2,6-Dibromo-4-nitroaniline" is China's quality standard for this compound, which is used to regulate its production, testing and application. This article will provide a detailed interpretation from multiple dimensions such as standard background, technical requirements, and testing methods.
Background of Standard Formulation and Technological Evolution
GB/T 23669-2016 replaces the previous GB/T 23669-2009 version. The main improvements include:
- Added ash control index: clarified the mass fraction of ash and its determination method.
- Modified appearance evaluation method: adjusted from visual observation to a more objective evaluation standard.
- Optimization of liquid chromatography detection conditions: The wavelength and mobile phase ratio were adjusted to improve detection accuracy.
Quality requirements and test methods
| Item | Indicator | Determination method |
|---|---|---|
| Appearance | Yellow powder | Visual method (5.2) |
| Purity of 2,6-dibromo-4-nitroaniline | ≥98.00% | Liquid chromatography method (5.3) |
| Content of 2,6-dichloro-4-nitroaniline | ≤0.05% | Liquid chromatography method (5.3) |
| Initial melting point of dry product | 200.0℃ | GB/T 2384 |
| Moisture mass fraction | ≤1.0% | Drying method (5.5) |
| Ash mass fraction | ≤0.20% | Ignition method (GB/T 21876) |
Implementation suggestions and precautions
1. Quality control: Manufacturers should strictly follow the standard requirements for raw material screening and process monitoring to ensure that the products meet the indicators in Table 1.
2. Inspection rules: In addition to factory inspection, it is recommended to conduct regular re-inspections, especially when there are large batch differences. During re-inspection, samples should be taken from double packaging to ensure the representativeness of the data.
3. Safety and storage: This compound has certain toxicity. Operators should wear protective equipment and ensure that the product is stored in a cool and dry environment, away from fire and high temperature areas.

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