GB/T 32329-2015 in English
VALIDTest method for oxidation resistance of oxynitride materials―Non-isothermal oxidation
- Issued on:2015-12-31
- Implemented on:2016-07-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
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《GB/T 32329-2015氮氧化物材料抗氧化性试验方法 变温氧化法》由TC415(全国产品回收利用基础与管理标准化技术委员会)归口,主管部门为国家标准化管理委员会。
本标准规定了用变温氧化法测试氮氧化物材料抗氧化性的原理、试验设备及仪器、试样、试验步骤、结果计算、评价指标及试验报告。
本标准适用于氮氧化物材料在高温条件下抗氧化性的测试和评价。
Introduction
Test method for oxidation resistance of nitrogen oxide materials: variable temperature oxidation method
The oxidation resistance of nitrogen oxide materials is an important indicator of their ability to resist oxidation in high temperature and oxidizing atmosphere. This standard provides a systematic test method through the variable temperature oxidation method to ensure the accuracy and repeatability of the test results.
Test principle and equipment requirements
| Project | Specific requirements |
|---|---|
| Heating furnace | The temperature difference in the constant temperature zone is ≤5℃, the maximum operating temperature is ≥1600℃, and it is equipped with a gas path system. |
| Analytical balance | Range 120g, sensitivity 0.0001g, data acquisition system updates 1200 times per second. |
| Temperature controller | Precision is 1.0 level to ensure the accuracy of temperature control. |
Test steps and data acquisition
The test process includes sample weighing, heating furnace heating, oxidation reaction monitoring and data analysis. By recording the mass change of the sample at different temperatures, the oxidation weight gain per unit area (G), the initial oxidation temperature (T1) and the maximum oxidation rate temperature (T2) are calculated. Data acquisition should ensure that the deviation of parallel samples does not exceed 5% to ensure the validity of the results.
Antioxidant performance evaluation indicators
The main evaluation indicators include oxidation weight gain per unit area, initial oxidation temperature and maximum oxidation rate temperature. These indicators are obtained by fitting the oxidation weight gain curve and its first-order differential curve to ensure a comprehensive evaluation of the material's antioxidant capacity.

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