GB/T 37167-2018 in English
VALIDParticle—Separation and measurement of trace magnetic materials(elements)in inorganic powder
- Issued on:2018-12-28
- Implemented on:2019-03-01
- File Format:PDF
- Delivery:Within 1 day
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《GB/T 37167-2018颗粒 无机粉体中微量和痕量磁性物质分离与测定》由TC168(全国颗粒表征与分检及筛网标准化技术委员会)归口,TC168SC1(全国颗粒表征与分检及筛网标准化技术委员会颗粒分会)执行,主管部门为国家标准化管理委员会。
Introduction
GB/T 37167—2018 Standard Interpretation
1. Standard Scope and Applicability
This standard is applicable to the determination of trace magnetic impurities in inorganic powders with a particle size not greater than $60~\mu\mathrm{m}$.
2. Separation and Extraction of Magnetic Substances
| Steps | Detailed Description |
|---|---|
| Magnetic Bar Preparation | Put the magnetic bar into a conical flask, add concentrated hydrochloric acid and heat to boiling, cool and clean it for later use. |
| Sample treatment | Weigh an appropriate amount of sample and place it in a sample jar, add a magnetic bar and dispersion medium, and shake to mix for 30-60 minutes. |
3. Determination of magnetic impurities
Case analysis:Testing of magnetic impurities in lithium iron phosphate.
- Weigh $200.30~\mathrm{g}$ lithium iron phosphate sample and separate the magnetic impurities.
- After dissolution, use ICP-AES to determine the content of Cr, Mn, Fe, Co, Ni, and Zn elements.

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