GB/T 38339-2019 in English
VALIDDetermination of phosphorus content in fluorescent brightener products
- Issued on:2019-12-31
- Implemented on:2020-11-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$97.00
《GB/T 38339-2019荧光增白剂产品中磷含量的测定》由TC134(全国染料标准化技术委员会)归口,主管部门为中国石油和化学工业联合会。
Introduction
Interpretation of the National Standard of the People's Republic of China GB/T 38339—2019
1. Background of the Standard
As an important auxiliary agent in the textile, washing and papermaking industries, the quality control of fluorescent brighteners is of vital importance. Phosphorus content is an important indicator to measure its performance and safety. The formulation of this standard aims to unify the test methods and ensure the accuracy and comparability of data.
2. Comparison of standard frameworks
| Content dimension | Wet digestion | Microwave digestion | Phosphomolybdenum blue method | Phosphomolybdenum yellow method |
|---|---|---|---|---|
| Scope of application | Widely applicable, suitable for complex samples | Efficient and fast, suitable for small batch samples | High sensitivity, suitable for low phosphorus content detection | Applicable to samples with high phosphorus content |
| Operation complexity | High | Medium | High | Low |
| Detection sensitivity | General | High | High | Low |
3. Analysis of technology evolution
This standard combines traditional wet digestion with modern microwave digestion technology, reflecting the innovative development of detection methods. The application of phosphomolybdenum blue method and phosphomolybdenum yellow method demonstrates the advantages of chemical colorimetry in trace analysis.
4. Implementation suggestions
4.1 Method selection
- Samples with low phosphorus content:The phosphomolybdenum blue method is recommended because of its high sensitivity and simple operation.
- Samples with high phosphorus content:The phosphomolybdenum yellow method is preferred, which is suitable for the detection of phosphorus content above 500 mg/kg.
- Batch sample processing: It is recommended to use microwave digestion technology to improve efficiency.
4.2 Personnel training
Operators should receive systematic training, focusing on the correct use of instruments and equipment and the preparation of standard solutions. It is recommended to conduct internal quality control drills regularly to ensure data reliability.
4.3 Quality control
- Blank test: A blank test should be performed simultaneously on each batch of samples to evaluate the accuracy of the experiment.
- Repeatability test: The difference between two parallel measurement results should be ≤2 mg/kg or not more than 10% of the average value.
- Instrument calibration: Regularly calibrate the wavelength of the spectrophotometer to ensure measurement accuracy.

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