GB/T 8039-2022 in English
VALIDDetermination of total sulfur of coking benzole products
- Issued on:2022-10-12
- Implemented on:2022-10-12
- File Format:PDF
- Delivery:Via email within 1~3 business days
$214.00
《GB/T 8039-2022焦化苯类产品全硫含量的测定方法》由TC469(全国煤化工标准化技术委员会)归口,TC469SC3(全国煤化工标准化技术委员会炼焦化学分会)执行,主管部门为国家标准化管理委员会。
Introduction
Key points of standard update and technological evolution
| Technical elements | 2009 version of spectrophotometry | 2022 version of ultraviolet fluorescence method |
|---|---|---|
| Detection principle | Nickel-aluminum reduction-colorimetry | High temperature pyrolysis + fluorescence detection |
| Maximum detection limit | 30mg/kg | 100mg/kg |
| Analysis time | 90-120 minutes | 5-10 minutes |
Technical requirements for testing instruments
Key equipment must meet the following requirements:
- UV fluorescence sulfur analyzer Equipped with a 1050℃ high-temperature cracking furnace and an online drying device
- Spectrophotometer should use a 667nm dedicated detection module and quartz cuvette
- Uniformly equipped with GH3039 nickel alloy reaction bottles (resistant to 5mol/L acidic environment)
Quality control implementation plan
Abnormal handling procedures
- When the repeatability>RSD10%:
① Check Whether the content of nickel-aluminum alloy meets the 50±5% standard
② Calibrate the empty adsorption value of isopropanol reagent - Fluorescence signal attenuation processing: clean quartz tube + update drying film

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