JJG 154-2012 in English
VALIDVerification regulation of standard capillary viscometer
- Issued on:2012-12-14
- Implemented on:2013-06-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$262.00
本规程适用于相对法测量标准毛细管黏度计的首次检定、后续检定和使用中检查。
Introduction
Key points of the revision of the regulations
| Revision content | 1979 edition | 2012 edition |
|---|---|---|
| Technical indicators | Only time repeatability is specified | New constant stability (0.20-0.70%) |
| Standard level | Includes second-class standards | Cancel relevant clauses of second-class standards |
| Environmental control | No clear humidity requirement | Humidity≤75%RH |
Key metrological characteristics of viscometer
Calculate the viscometer constant according to the formula C=ν/t:
- The inner diameter of the capillary is divided into 8 grades (0.45-6.9mm)
- Time repeatability requirement ≤0.2%
- Constant reproducibility ≤0.3%
Verification operation specifications
Selection of standard materials
It is necessary to use National first-level standard viscosity fluid, and the viscosity range corresponding to different inner diameters is:
- 0.45mm capillary: 2mm²/s (double batch number)
- 6.9mm capillary: 30000-40000mm²/s
Constant temperature control requirements
| Temperature fluctuation | ≤±0.005℃/8h |
| Temperature field uniformity | ≤0.01℃ |
Implementation suggestions
Abnormal handling process
- Single out-of-tolerance data: take the average of 5 times after elimination
- Double out-of-tolerance data: need to be cleaned and re-calibrated
- Stability exceeds the standard: re-inspect after traceability analysis
Maintenance points
Cleaning must meet the standard of no water droplets on the inner wall, and the drying temperature shall not exceed 120℃. Recommendations for high-precision measurements:
- 0.45mm capillary: outflow time ≥ 600s
- Establish a 4-year period stability profile

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