NB/SH/T 0230-2019 in English
VALIDDetermination of composition in Vquefied petroleum gases勿gas chromatography
- Issued on:2019-06-04
- Implemented on:2019-10-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$214.00
Introduction
Analysis of the core content of the standard
| Technical elements | 1992 edition | 2019 edition | Improvement significance |
|---|---|---|---|
| Scope of application | C1-C5 pure hydrocarbons | Pure hydrocarbons + oxygen-containing compounds (dimethyl ether, etc.) | Adapt to the detection needs of new fuels |
| Injection method | Water bath vaporization | Liquid valve/flash evaporator | Improve injection accuracy |
| Chromatographic system | Single column and single valve | Dual system configuration | Achieve full component analysis |
Key technological breakthroughs
The standard innovatively adopts a combination of Al2O3 capillary column and Lowox polar column:
- System 1: 30m Al2O3 column to achieve complete separation of C1-C5 hydrocarbons
- System 2: Add 10m Lowox column, can detect dimethyl ether (1-40%), methanol (0.01-1%) and other oxygen-containing compounds
Implementation points
Quality control requirements
- Calibration samples must be prepared in accordance with the weighing method of GB/T 5274
- Liquid valve injection RSD <3%, flash evaporator injection RSD <4%
- Calibration curve for oxygen-containing compounds R2≥0.990
Safety precautions
When detecting samples containing dimethyl ether, it is necessary to use inertized cylinders to avoid the risk of leakage due to swelling of rubber seals.
Application Scenario Analysis
| Detection Type | Typical Components | Related Standards |
|---|---|---|
| Automotive LPG | C3-C4 Hydrocarbons | GB 19159 |
| Blended Dimethyl Ether | Dimethyl Ether + Hydrocarbons | GB 11174 |
| MTBE Process Gas | Methanol/MTBE+C4 | Process Control |

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