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NB/SH/T 0230-2019 in English

NB/SH/T 0230-2019 in English

VALID

Determination of composition in Vquefied petroleum gases勿gas chromatography

  • Issued on:2019-06-04
  • Implemented on:2019-10-01
  • File Format:PDF
  • Delivery:Via email within 1~3 business days
Price(USD): $220.00
$214.00
Standard No: NB/SH/T 0230-2019
Document status: VALID
Title in English: Determination of composition in Vquefied petroleum gases勿gas chromatography
Title in Chinese: 液化石油气组成的测定 气相色谱法
Language: English
File Format: Electronic (PDF)
Delivery: Via email within 1~3 business days
Issued on: 2019-06-04
Implemented on: 2019-10-01
Superseding: SH/T 0230-1992 Determination method for composition of liquefied petroleum gas (chromatography method )
Professional Classification: NB-Energy
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Introduction

Analysis of the core content of the standard

Technical elements 1992 edition 2019 edition Improvement significance
Scope of application C1-C5 pure hydrocarbons Pure hydrocarbons + oxygen-containing compounds (dimethyl ether, etc.) Adapt to the detection needs of new fuels
Injection method Water bath vaporization Liquid valve/flash evaporator Improve injection accuracy
Chromatographic system Single column and single valve Dual system configuration Achieve full component analysis

Key technological breakthroughs

The standard innovatively adopts a combination of Al2O3 capillary column and Lowox polar column:

  1. System 1: 30m Al2O3 column to achieve complete separation of C1-C5 hydrocarbons
  2. System 2: Add 10m Lowox column, can detect dimethyl ether (1-40%), methanol (0.01-1%) and other oxygen-containing compounds

Implementation points

Quality control requirements

  • Calibration samples must be prepared in accordance with the weighing method of GB/T 5274
  • Liquid valve injection RSD <3%, flash evaporator injection RSD <4%
  • Calibration curve for oxygen-containing compounds R2≥0.990

Safety precautions

When detecting samples containing dimethyl ether, it is necessary to use inertized cylinders to avoid the risk of leakage due to swelling of rubber seals.


Application Scenario Analysis

Detection Type Typical Components Related Standards
Automotive LPG C3-C4 Hydrocarbons GB 19159
Blended Dimethyl Ether Dimethyl Ether + Hydrocarbons GB 11174
MTBE Process Gas Methanol/MTBE+C4 Process Control

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