NB/SH/T 0951-2017 in English
VALIDStandard test method for particle size distribution of catalytic crackng catalyst by laser light scattering
- Issued on:2017-12-27
- Implemented on:2018-06-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$117.00
Introduction
Analysis of the core content of the standard
This standard uses a laser particle size analyzer to determine the particle size distribution of catalytic cracking catalysts. The main technical features include:
- Measurement range: 1-300μm particle size (median particle size 60-110μm)
- Theoretical model: Combined application of Mie scattering and Fraunhofer diffraction theory
- Precision index: Median particle size repeatability ≤2.6μm, reproducibility formula calculation
Comparative analysis of international standards
| Comparison dimensions | ASTM D4464-15 | NB/SH/T 0951-2017 |
|---|---|---|
| Particle size range | Not clearly defined | 1-300μm |
| Precision expression | Single index | Four index system (including cumulative volume fraction) |
| Instrument requirements | General type | Appendix A specifies reference conditions |
Key technical points
Optical model selection principles
For particles with a median particle size of less than 20μm, it is mandatory to use the Mie scattering theory and the following must be entered:
- The real part of the complex refractive index (such as 1.53 for kaolin)
- The imaginary part of the absorption value (usually 0.01 for metal oxides)
Interference control measures
- Bubble interference: Visually confirm that there are no bubbles when circulating the dispersant
- Contaminant treatment: Pre-clean with a compatible solvent
- Agglomeration prevention: Ultrasonic dispersion power control (Appendix A specifies a maximum power of 90%)
Implementation recommendations
Laboratory operating specifications
- Sampling strictly follows the NB/SH/T 0960 standard
- After the instrument is preheated, it is necessary to perform optical path calibration (refer to JJF 1211)
- The background value should be controlled within the manufacturer's requirements
Notes on data reporting
- The refractive index parameter used must be indicated
- The median particle size should be rounded to one decimal place
- Abnormal data should be marked with the measured shading rate (8-18% is recommended)

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