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particle size distribution median particle size 1-300μm particle size laser particle size analyzer 0951-2017 particle size range upland cotton scopethis standard content-na2 edta titration method scopethis standard deliquescent mud
NB/SH/T 0951-2017 in English

NB/SH/T 0951-2017 in English

VALID

Standard test method for particle size distribution of catalytic crackng catalyst by laser light scattering

  • Issued on:2017-12-27
  • Implemented on:2018-06-01
  • File Format:PDF
  • Delivery:Via email within 1~3 business days
Price(USD): $120.00
$117.00
Standard No: NB/SH/T 0951-2017
Document status: VALID
Title in English: Standard test method for particle size distribution of catalytic crackng catalyst by laser light scattering
Title in Chinese: 催化裂化催化剂粒度分布的测定 激光散射法
Language: English
File Format: Electronic (PDF)
Delivery: Via email within 1~3 business days
Issued on: 2017-12-27
Implemented on: 2018-06-01
Professional Classification: NB-Energy
Related Keywords: particle size distribution
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1-300μm particle size
laser particle size analyzer
0951-2017 particle size range
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Introduction

Analysis of the core content of the standard

This standard uses a laser particle size analyzer to determine the particle size distribution of catalytic cracking catalysts. The main technical features include:

  • Measurement range: 1-300μm particle size (median particle size 60-110μm)
  • Theoretical model: Combined application of Mie scattering and Fraunhofer diffraction theory
  • Precision index: Median particle size repeatability ≤2.6μm, reproducibility formula calculation

Comparative analysis of international standards

Comparison dimensions ASTM D4464-15 NB/SH/T 0951-2017
Particle size range Not clearly defined 1-300μm
Precision expression Single index Four index system (including cumulative volume fraction)
Instrument requirements General type Appendix A specifies reference conditions

Key technical points

Optical model selection principles

For particles with a median particle size of less than 20μm, it is mandatory to use the Mie scattering theory and the following must be entered:

  1. The real part of the complex refractive index (such as 1.53 for kaolin)
  2. The imaginary part of the absorption value (usually 0.01 for metal oxides)

Interference control measures

  • Bubble interference: Visually confirm that there are no bubbles when circulating the dispersant
  • Contaminant treatment: Pre-clean with a compatible solvent
  • Agglomeration prevention: Ultrasonic dispersion power control (Appendix A specifies a maximum power of 90%)

Implementation recommendations

Laboratory operating specifications

  1. Sampling strictly follows the NB/SH/T 0960 standard
  2. After the instrument is preheated, it is necessary to perform optical path calibration (refer to JJF 1211)
  3. The background value should be controlled within the manufacturer's requirements

Notes on data reporting

  • The refractive index parameter used must be indicated
  • The median particle size should be rounded to one decimal place
  • Abnormal data should be marked with the measured shading rate (8-18% is recommended)

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