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quinoline content active agents determination agents introduction gb/t trace quinoline core determination principle industrial sodium steam convection content titrimetric method scopethis part
GB/T 37505-2019 in English

GB/T 37505-2019 in English

VALID

Surface active agents—Determination of quinoline content in dispersing agents

  • Issued on:2019-06-04
  • Implemented on:2020-05-01
  • File Format:PDF
  • Delivery:Via email within 1~3 business days
Price(USD): $100.00
$97.00
Standard No: GB/T 37505-2019
Document status: VALID
Title in English: Surface active agents—Determination of quinoline content in dispersing agents
Title in Chinese: 表面活性剂 分散剂中喹啉含量的测定
Language: English
File Format: Electronic (PDF)
Delivery: Via email within 1~3 business days
Issued on: 2019-06-04
Implemented on: 2020-05-01
ICS Classification: 71.100.40-Surface active agents
Chinese Classification: G72-Basic standards and general methods for surface active agent
Professional Classification: GB-National Standard
Related Keywords: quinoline content
active agents determination
agents introduction gb/t
trace quinoline
core determination principle
Related Topics: mid-range dispersion
Quinoline content detection
Active bromine content
Secondary dispersant Main dispersant
Dosage content exceeds
Dispersed
Surfactant detection
agent dispersion
GBT37505
GB/T 37505-2019
Surfactant
Classification and application of fluorinated surfactants
Determination of sodium chloride in surfactants
Quinoline test
Method for determination of surfactant dispersion power

《GB/T 37505-2019表面活性剂 分散剂中喹啉含量的测定》由TC63(全国化学标准化技术委员会)归口,TC63SC8(全国化学标准化技术委员会(特种)界面活性剂分会)执行,主管部门为中国石油和化学工业联合会。


Introduction

GB/T 37505—2019: In-depth interpretation of the standard for determination of quinoline content in surfactant dispersants

I. Background and significance of standard formulation

GB/T 37505—2019 "Determination of quinoline content in surfactant dispersants" is an important standard in China's chemical industry, mainly used for the detection of quinoline content in dispersants produced from coal chemical raw materials. This standard fills the gap in the domestic detection method of trace quinoline in dispersants and provides a scientific basis for product quality control.


II. Core determination principle and technical route

Technical parameters Gas chromatography (GC-FID) Gas chromatography-mass spectrometry (GC-MS)
Detection sensitivity Detection limit: 20 mg/kg Detection limit: 5 mg/kg
Analysis time About 15 minutes/time About 20 minutes/time
Scope of application Routine detection Arbitration inspection and complex samples

III. Key technical points for the implementation of the standard

Requirements for reagents:The chemical reagents used in the test must comply with national standards, and the test water must meet the third-grade water specifications in GB/T 6682.

Instrument configuration:Equipped with a gas chromatograph (GC-FID) or a gas chromatograph-mass spectrometer (GC-MS), and meet the corresponding technical index requirements.

Sample pretreatment:Weigh 0.5 g of sample, dissolve it in water, add ethyl acetate to extract quinoline, and centrifuge to separate the organic phase for analysis.


IV. Scope and limitations of the standard

Scope of application:Applicable to the determination of quinoline content in various surfactant-type dispersants produced from coal chemical raw materials.

Limitations:This standard is mainly aimed at the coal chemical industry, and the pretreatment conditions may need to be adjusted for other types of dispersants.


V. Implementation recommendations and precautions

Case study: Practical application in the laboratory

A coal chemical enterprise adopted the GB/T 37505-2019 standard to control the quality of dispersant products. In the experiment, they found the following key points:

  • During sample pretreatment, ultrasonic-assisted extraction can significantly improve the extraction efficiency of quinoline.
  • The GC-MS method has more advantages in the detection of quinoline in complex matrices.
  • It is recommended to recalibrate the standard curve once a month to ensure accuracy.

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