GB/T 37505-2019 in English
VALIDSurface active agents—Determination of quinoline content in dispersing agents
- Issued on:2019-06-04
- Implemented on:2020-05-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$97.00
《GB/T 37505-2019表面活性剂 分散剂中喹啉含量的测定》由TC63(全国化学标准化技术委员会)归口,TC63SC8(全国化学标准化技术委员会(特种)界面活性剂分会)执行,主管部门为中国石油和化学工业联合会。
Introduction
GB/T 37505—2019: In-depth interpretation of the standard for determination of quinoline content in surfactant dispersants
I. Background and significance of standard formulation
GB/T 37505—2019 "Determination of quinoline content in surfactant dispersants" is an important standard in China's chemical industry, mainly used for the detection of quinoline content in dispersants produced from coal chemical raw materials. This standard fills the gap in the domestic detection method of trace quinoline in dispersants and provides a scientific basis for product quality control.
II. Core determination principle and technical route
| Technical parameters | Gas chromatography (GC-FID) | Gas chromatography-mass spectrometry (GC-MS) |
|---|---|---|
| Detection sensitivity | Detection limit: 20 mg/kg | Detection limit: 5 mg/kg |
| Analysis time | About 15 minutes/time | About 20 minutes/time |
| Scope of application | Routine detection | Arbitration inspection and complex samples |
III. Key technical points for the implementation of the standard
Requirements for reagents:The chemical reagents used in the test must comply with national standards, and the test water must meet the third-grade water specifications in GB/T 6682.
Instrument configuration:Equipped with a gas chromatograph (GC-FID) or a gas chromatograph-mass spectrometer (GC-MS), and meet the corresponding technical index requirements.
Sample pretreatment:Weigh 0.5 g of sample, dissolve it in water, add ethyl acetate to extract quinoline, and centrifuge to separate the organic phase for analysis.
IV. Scope and limitations of the standard
Scope of application:Applicable to the determination of quinoline content in various surfactant-type dispersants produced from coal chemical raw materials.
Limitations:This standard is mainly aimed at the coal chemical industry, and the pretreatment conditions may need to be adjusted for other types of dispersants.
V. Implementation recommendations and precautions
Case study: Practical application in the laboratory
A coal chemical enterprise adopted the GB/T 37505-2019 standard to control the quality of dispersant products. In the experiment, they found the following key points:
- During sample pretreatment, ultrasonic-assisted extraction can significantly improve the extraction efficiency of quinoline.
- The GC-MS method has more advantages in the detection of quinoline in complex matrices.
- It is recommended to recalibrate the standard curve once a month to ensure accuracy.

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