GB/T 38729-2020 in English
VALIDSurface active agents—Test methods of technical sodium primary alkylsulphates
- Issued on:2020-04-28
- Implemented on:2020-11-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$156.00
《GB/T 38729-2020表面活性剂 工业伯烷基硫酸钠试验方法》由TC272(全国表面活性剂和洗涤用品标准化技术委员会)归口,主管部门为中国轻工业联合会。
Introduction
Interpretation of the core content of the standard
| Test items | Method basis | Technical improvement |
|---|---|---|
| pH value determination | GB/T 6368 | Measured using 10% solution, sample is unstable when pH < 7 |
| Petroleum ether extractables | Appendix A | Increase the number of extractions to 5 times, and clarify the temperature control requirements |
| Fatty alcohol content | Appendix B | Optimize the acid hydrolysis reflux time to 4 hours |
Key technical differences
Main improvements of this standard compared with ISO 894:1977:
- Ethanol concentration is adjusted to 95% (not specified in the original standard)
- Sodium chloride determination is changed to GB/T 3050 potentiometric titration method
- Acetone is added as washing solvent
Key points of experimental operation
Key steps of petroleum ether extraction
- Sample dissolution needs to be maintained in a 70℃ water bath
- Ethanol is added to demulsify during stratification
- The residue needs to be dried with controlled air flow at 30℃
Implementation suggestions
Laboratories should pay attention to:
- When the water content is greater than 5%, azeotropic distillation is preferred
- Before determining the total alkalinity, it is necessary to confirm that the pH is greater than 7 and the free base is greater than 0.3
- Ether extraction must be performed in a fume hood

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