GB/T 39540-2020 in English
VALIDFast determination of shale gas composition—Laser Raman spectroscopy
- Issued on:2020-11-19
- Implemented on:2021-06-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$117.00
《GB/T 39540-2020页岩气组分快速分析 激光拉曼光谱法》由TC244(全国天然气标准化技术委员会)归口,主管部门为国家标准化管理委员会。
Introduction
Interpretation of the core content of the standard
This standard establishes the technical specifications for the determination of the main components of shale gas by laser Raman spectroscopy. Its innovation is reflected in:
| Technical elements | GB/T 39540-2020 requirements | Comparison with traditional chromatography |
|---|---|---|
| Analysis speed | Real-time detection (response in seconds) | 10-30 minutes/sample |
| Detection limit | 0.01% mole fraction | 0.001% mole fraction |
| Applicable components | CH4/C2H6/CO2, etc. | Full component analysis |
Key instrument configuration requirements
The standard puts forward clear technical indicators for Laser Raman gas analyzer:
- Laser: power ≥0.5W, annual fluctuation <±5%
- Detection module: resolution ≤7cm-1, thermal drift <0.1cm-1/℃
- Sampling system: filtration accuracy 0.1μm
Application case: On-site detection of shale gas fields
A shale gas platform in Sichuan uses the LRS-3000 laser analyzer to achieve continuous monitoring of CH4 content (85-98%), with a data deviation of <1.2%, which is 20 times more efficient than traditional methods.
Calibration system construction
Standard three-level calibration system:
- Zero calibration: Use 99.999% high-purity inert gas
- Benchmark calibration: 5%CO2/Ar and other binary mixed gases
- Working calibration: Concentration matches the actual sample
Implementation suggestions
Operational precautions:
| Risk points | Solutions |
|---|---|
| Laser power attenuation | Energy calibration before daily startup |
| Cross interference | Update the interference factor matrix regularly |
| Sample contamination | Replace the filter module every 50 tests |

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