GB/T 18606-2017 in English

SUPERSEDED

The test method for biomarkers in sediment and crude oil by GC-MS

Issued on:2017-05-12
Implemented on:2017-12-01
File Format:PDF
Delivery:Via email within 5 business days

Price(USD)： $220.00
$214.00

Standard No:	GB/T 18606-2017
Document status:	SUPERSEDED
Superseded by:	GB/T 18606-2025 Determination of biomarkers in sediment and crude oil by gas chromatography-mass spectrometry
Superseded on:	2026-05-01
Title in English:	The test method for biomarkers in sediment and crude oil by GC-MS
Title in Chinese:	气相色谱-质谱法测定沉积物和原油中生物标志物
Language:	English
File Format:	Electronic (PDF)
Delivery:	Via email within 5 business days
Issued on:	2017-05-12
Implemented on:	2017-12-01
Superseding:	GB/T 18606-2001 The standard test method for biomarker in sediment and crude oil by GC-MS
ICS Classification:	75.040-Crude petroleum
Chinese Classification:	E21-Crude petroleum
Professional Classification:	GB-National Standard
Related Keywords:	crude oil crude oil sample c31 hopane dimerspeak height ratio method precisionrepeatabilityr=0.0047+0.0125mgb/t oil field test method
Related Topics:	Biomass Spectrometry Gas Chromatography-Mass Spectrometry Biomass Spectrometry mass spectrum base peak Biomarkers sediment oil MS standard gas gas chromatography substance gas chromatography mass spectrometry Microbial Mass Spectrometry Purity of substances in chromatography mass spec biological GC-MS biomarkers Atomic Gas Chromatography Gas chromatography mass spectrometry oil Crude Oil Biomarkers What does gas chromatography mass spectrometry analyze? Mass Spectrometry Microbial Methods mass spec biological Chromatographic peak Principle of original dichroism Chromatogram peak Biomarker detection Biomarker detection biomarker Chromatogram peak+ Determination of Biomarkers in Sediments and Crude Oil by Gas Chromatography-Mass Spectrometry Biomarker Test Samples GC volume gas phase reference material Mass spec relative to atom Mass spectrum + base peak Gas Chromatography Polar Substances Gas Chromatography Standard Material Principle of Chromatography Sediment Dry Matter GC volume fraction Gas phase substance detection mass spectrometer GC volume fraction Principle of Chromatography gas chromatography mass spectrometry GC volume gas chromatography substance Spectrum material Gas Chromatography Product Peak Sediment detection biological mass spectrometry method bioenergy spectrum mass spectrometry gas phase How to Integrate Chromatographic Peaks biomarker Chromatographic standard external standard Biomass Spectrometry Chromatographic generation Product mass spectrometry detection Chromatographic generation The generation of chromatography Assign chromatographic source Over the spectrum biological Derivatization in Gas Chromatography mass spectrum peak headspace gas chromatography Principles of Chromatography 1 Atomic Gas Chromatography Spectrum Bio Chromatography produced Chromatogram peak Sediment detection ge, oil chromatography Biomarker mass spectrometry Spectrum Bio Biological sample mass spectrometry multiple biomarkers Mass Spectrometry Biomarkers biological spectroscopy Gas phase peak material Chromatography of biological samples Fenghua Biomass Spectrometry sediment dating gas phase of polymer Marker Mass Spectrum oil chromatography Gas Chromatography Mass Spectrometry Derivatization Spectrometer deposits mass spectrometry biological Methods of Sediment Dating Biomarkers? Automatic Chromatography Integration Principles of Normal Phase Chromatography Principle of Normal Phase Chromatography dna biomarker dna biomarker Gas Chromatography Standard Material Biomarker Non-Targeted gas phase reference material Microbial mass spectrometry+ oil in water Atomic Gas Chromatography Principles of Chromatography Gas chromatography + reference material The origin of chromatography, i Method for Determination of pH in Sediment Biomarker Non-Targeted Novel Biomarkers chromatography substance ge oil chromatography Gas Chromatography Mass Spectrometry Derivatization Principle of Size Chromatography Oleic acid gas chromatography Gas Chromatography Standard External Standard What substance is spectroscopically Gas Chromatography + Mass Spectrometry positive biomarker Chromatographic marker peak Gas chromatography biological detection Biomarker Panel Chromatography Atomic Emission Chromatography Gas in Petroleum in Gas Chromatography Material gas phase peak mass spectrometer Automatic Chromatography Integration Chromatographic peak principle External Standard for Mass Spectrometry Biomarker detection method gas chromatography oil Chromatography sampler principle Quantification by Gas Chromatography Derivatization GC and GC-MS Chromatographic compounds specific biomarkers Standard substance for mass spectrometry Gas chromatography standard + external standard method Biomass Spectrometry,,, Determination of Benzene Series in Air by Gas Chromatography object mark mass chromatographic peak GC peak volume Modern Sediment Gas Chromatography-Mass Spectrometry According to biological seven mass spectrometry Microbial mass spectrometry in water Chromatographic peak co-elution Gas Chromatography + Substance Chromatographic cell volume Gas Chromatography Polar Substances Principle of head-on chromatography GC-MS derivatization Eco Center Mass Spectrometry Sediment in the liquid Automatically Integrate Chromatography Derivatization in GC-MS Raw material phase Biophase index Main Derivatization Methods in Gas Chromatography mass spectrometry biological mass spectrometry Gas Chromatography Substances Abnormal biomarkers Biomarker Identification Methods Biomass Spectrometry Mass Spectrometry How to integrate the chromatogram Microbial mass spectrometry method comparison Principles of Polymer Chromatography How Normal Phase Chromatography Works Biomass Spectrometry Products DNA biomarkers GBT18606 GB/T 18606-2001 GB/T 18606-2017 biochromatography Biomarker Validation Sediment Physical Properties The basis for judging the purity of substances by gas chromatography Gas chromatography for detection of mineral oil in edible oil Principles of gas phase mass spectrometry Chromatography does not automatically integrate Biochemical Chromatography Network Biomarker Validation Methods Principles of size exclusion chromatography Physical vapor deposition method steps Medium I crude oil Principle of x500r mass spectrometry Selection of internal standard substances for gas chromatography Spectrum Biotechnology Zhao Yuan Dead volume in gas chromatography Features of bio-inert liquid chromatography lipid biomarkers GOW-MaC816 gas chromatography principle Reasons for incorrect gas chromatography data Meiji Biomass Spectrometry Antu microbial mass spectrometer Color scale in standard material Gas chromatography reduces peak area of substances Principles of affinity chromatography Crude oil standard gas chromatography Material standard hydrogen spectrum Gas chromatography mass spectrum of gasoline standard sample Microbial mass spectrometry Oxygen mass spectrum standard spectrum Gas Chromatography Column Regeneration Methods Chromatography principles and methods Gas chromatography material standard curve Biomass gasification related Sediment Testing Standards Determination of petroleum in sediments Sediment Arsenic Standard Current methods for detecting biomarkers Statistical methods for biomarker prediction of eclampsia Netdisk Biomass Spectrometry Technology and Methods Microbial mass spectrometry charges Mineral oil quality in sediments Biomarker Research Methods Chromatographic standard gas sediment petroleum Standard gases for oil chromatography Chromatographic System Integration Method Gas chromatograph area calculation method National standard determination method for total nitrogen in sediments Biochromatography and affinity separation methods Biomarker detection method development Machine learning biomarker methods oil change chromatography Microbial mass spectrometry quality gb18606 gb/t 18606 gb/t 18606-2017

《GB/T 18606-2017气相色谱-质谱法测定沉积物和原油中生物标志物》由TC355（全国石油天然气标准化技术委员会）归口，TC355SC3（全国石油天然气标准化技术委员会石油地质勘探分会）执行，主管部门为国家标准化管理委员会。

Introduction

Standard Technology Evolution and Core Upgrade

Dimensions	2001 Edition	2017 Edition Upgrade Content
Detection Compounds	Basic Tricycloalkanes, Hopanes	7 New Compounds: Bicyclic Sesquiterpenes, Polycyclic Aromatic Hydrocarbons, etc.
Chromatogram Specifications	Appendix B has fewer diagrams	Add 8 types of mass chromatograms (Figures B.1-B.8)
Mass Spectrometer Parameters	Scanning Mass Number ≥500	Explicitly require ≥650amu

Technical requirements for key instruments

The core equipment Gas Chromatography-Mass Spectrometer must meet the following requirements:

EI ion source electron energy70eV
Capillary column stationary phase is 5% benzylsiloxane
Carrier gas purity ≥99.99% nitrogen

Compound identification system

Typical application case: The following were detected in a crude oil sample from an oil field:

The m/z 191 chromatogram shows that the C₃₁ hopane (22S/22R) peak separation is 92%
m/z 217 spectrum successfully identified ααα-C₂₉sterane (20R)

Quality Control Requirements

Indicators	Requirements	Detection Methods
Resolution	Complete Separation of C₃₁ Hopane Dimers	Peak Height Ratio Method
Precision	Repeatabilityr=0.0047+0.0125m	GB/T 6379.1

Implementation Suggestions

Operational precautions:

During tuning, ensure that the peak height of m/z 69 is 100% and the peak height of m/z 219 is 40-80%
For aromatic analysis, a 3℃/min gradient temperature increase is recommended
For highly mature samples, focus on the sterane 20S/20R separation

More samples: DL/T 368-2010 JGJ 94-2008 DL/T 5154-2012

Sample only — not a preview of GB/T 18606-2017

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