GB/T 38602-2020 in English
VALIDTest method of catalytic activity for catalytic wet oxidation of organic wastewater
- Issued on:2020-03-31
- Implemented on:2021-02-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$97.00
《GB/T 38602-2020湿式催化氧化有机废水催化剂活性试验方法》由TC63(全国化学标准化技术委员会)归口,TC63SC10(全国化学标准化技术委员会化工催化剂分会)执行,主管部门为中国石油和化学工业联合会。
Introduction
Analysis of the core content of the standard
| Technical elements | GB/T38602-2020 requirements | Conventional methods in the industry |
|---|---|---|
| Test object | COD removal rate of phenol wastewater | Mixed wastewater of various organic substances |
| Reaction conditions | 180℃±2℃/2.0MPa | 150-220℃/1.5-3.0MPa |
| Parallelism requirements | Range value ≤3% | Usually ≤5% |
Key Technical Points
Test Principle:The COD removal rate is measured by the oxidation of phenol (C6H5OH) to CO2 and H2O under the action of oxygen to characterize the catalyst activity.
Device Requirements:The TA10 titanium reactor is used, which must meet the parameters of 500mL volume, 10MPa pressure resistance, 300℃ temperature resistance, etc., and equipped with a magnetic coupling stirring system (1200r/min).
Implementation precautions
- Safety protection: Phenol is a toxic substance. The test must be carried out in a fume hood equipped with emergency eyewash and fire extinguishing equipment
- Sample preparation: The catalyst needs to be ground to <75μm and dried at 110℃ for 5 hours before use
- Gas replacement: Strictly carry out nitrogen-oxygen replacement three times to prevent explosion risks
Standard evolution background
This standard was jointly drafted by Xi'an Kaili New Materials and other five units, filling the gap in the activity evaluation method of wet catalytic oxidation catalysts. Compared with the traditional biodegradation method, this method has the characteristics of high treatment efficiency (1h to complete the test) and a wide range of applications (including benzene ring organic matter).
Typical Application Cases
A petrochemical enterprise used Pd/CeO2 catalyst to treat phenol-containing wastewater. According to the test results of this standard, the COD removal rate reached 92%, which is 3 times higher than that of non-catalytic oxidation treatment.

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