GB/T 39665-2020 in English
VALIDDetermination of 55 banned pesticides residues in cosmetics containing plant extracts
- Issued on:2020-12-14
- Implemented on:2021-07-01
- File Format:PDF
- Delivery:Via email within 5 business days
$301.00
《GB/T 39665-2020含植物提取物类化妆品中55种禁用农药残留量的测定》由TC374(全国质量监管重点产品检验方法标准化技术委员会)归口,主管部门为国家标准化管理委员会。
Introduction
Analysis of the core content of the standard
| Detection dimensions | Liquid chromatography-tandem mass spectrometry (20 types) | Gas chromatography-mass spectrometry (35 types) |
|---|---|---|
| Applicable matrix | Lotion/emulsion/cream/mask | |
| Pretreatment | Acetonitrile extraction + gel permeation chromatography purification | |
| Detection limit range | 0.0005-0.05 mg/kg | 0.02-0.1 mg/kg |
Key Technical Points
Optimization of Extraction Process:For viscous samples such as creams, the standard specifically recommends adding 5mL of water to disperse before extracting with acetonitrile. This operation can improve the separation efficiency of the centrifuge.
Dual Platform Detection:LC-MS/MS uses 0.1% formic acid water-acetonitrile gradient elution for 20 pesticides such as carbaryl; GC-MS uses 5% phenyl-methylpolysiloxane columns for 35 pesticides such as aldrin.
Implementation suggestions
- Standard solutions should be prepared and used immediately, and stored at -18°C away from light
- For cream samples, it is recommended to add a water dispersion step
- Pay attention to the matrix effect of compounds such as epoxiconazole in LC-MS/MS

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