GB/T 9491-2021 in English
VALIDFlux for tin soldering
- Issued on:2021-12-31
- Implemented on:2022-07-01
- File Format:PDF
- Delivery:Via email within 5 business days
$418.00
《GB/T 9491-2021锡焊用助焊剂》由TC47(全国印制电路标准化技术委员会)归口,主管部门为工业和信息化部(电子)。
Introduction
Standard Evolution and Industry Significance
GB/T9491-2021, as a new standard replacing the 2002 version, adapts to the industry trend of popularization of lead-free solder and miniaturization of electronics. The newly added requirements of electrochemical migration test and PCB ion residue detection directly respond to the stringent requirements of high-density integrated circuits on soldering reliability.
Core classification system
| Classification dimensions | 2002 edition | 2021 edition | Technological breakthroughs |
|---|---|---|---|
| Morphological classification | Liquid only | Liquid()/Solid(S)/Paste(P) | Covering SMT mounting process requirements |
| Activity grading | Level 3 (L/M/H) | Level 5 (0/1M/0M/1H/0H) | Precise control of halogen content |
| Material type | Rosin type | Class 4 (RO/RE/OR/IN) | Adapt to the development of environmentally friendly materials |
Analysis of key technical requirements
5.8 Solderability index
Expansion rate requirements are significantly improved: Lead-free solder is increased from 65% in the 2002 version to 70-80%, verified by the copper plate solder ring test method specified in 6.9.1. In actual applications, after a communication equipment manufacturer used ROM1 type flux, the QFN package soldering yield increased by 12%.
5.13 Electrochemical Migration (ECM)
New test items are added, requiring that after 168h aging:
1) Insulation resistance ≥ 10% of the initial value
2) Conductor spacing reduction ≤ 20%
Verified by the 0.318mm gap comb circuit shown in Figure 3 to prevent the risk of short circuit caused by ion migration in vehicle electronics.
Innovative detection methods
6.10.2.2 Ion chromatography
Compared with the traditional silver chromate test paper method, the Cl/Br/F ion content can be accurately detected to 0.0005%. After adopting this method, the halogen control accuracy of a certain aerospace-grade flux has been improved by 3 orders of magnitude.
6.17 Splash test
The amount of solder wire splash is quantitatively evaluated through the dedicated device in Figure 4 to solve the problem of solder ball contamination in consumer electronics assembly. Actual measurements show that when the Fs value is controlled at ≤0.3%, it can meet most precision assembly requirements.
Implementation recommendations
- Material switching: When transitioning from traditional rosin type (RO) to resin type (RE), it is necessary to simultaneously verify the acid value (6.8) and copper mirror corrosion (6.12) performance
- Process adjustment: The viscosity of paste flux (P) should be tested according to 6.5 before use, and it is recommended to maintain 800-1200cps at 20℃
- Quality control: It is recommended to add 5.15 PCB ion residue batch inspection, and use the megohmmeter method to ensure that the NaCl equivalent is <1.56μg/cm²

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