GB/T 40407-2021 in English

VALID

X-ray powder diffraction analysis method for determining the phases in portland cement clinker

Issued on:2021-08-20
Implemented on:2022-03-01
File Format:PDF
Delivery:Via email within 1~3 business days

Price(USD)： $220.00
$214.00

Standard No:	GB/T 40407-2021
Document status:	VALID
Title in English:	X-ray powder diffraction analysis method for determining the phases in portland cement clinker
Title in Chinese:	硅酸盐水泥熟料矿相X射线衍射分析方法
Language:	English
File Format:	Electronic (PDF)
Delivery:	Via email within 1~3 business days
Issued on:	2021-08-20
Implemented on:	2022-03-01
ICS Classification:	91.100.10-Cement. Gypsum. Lime. Mortar
Professional Classification:	GB-National Standard
Related Keywords:	x-ray powder diffraction analysis method core analysis methods analysis dimension traditional method first special analysis method standard quantitative x-ray diffraction analysis standard method resolution single peak analysis
Related Topics:	x-ray diffraction x-ray diffraction group X-ray Diffraction Standards x-diffraction X-ray Diffraction Analysis x-ray Diffraction analysis Ray standard x-ray diffraction Ray Diffraction Diffraction peak intensity diffraction Diffraction method X-ray Diffraction+ Standard Diffraction peaks X-ray analysis device Is X-ray Diffraction Safe? Transmission Diffraction X-ray Diffraction Quantitative Analysis x-ray standard copper silicon x-ray x-ray diffraction method X-ray Diffraction Quantitative Analysis Portland cement x-ray Liquid phase analysis salt Diffraction peaks Zero Diffraction Silicon Standard Diffraction of Silicon X-ray diffraction sample preparation Diffraction peak analysis x-ray diffraction reverse zero diffraction x+ ray diffraction x-ray diffraction particle size Diffraction analysis Why X-ray Diffraction X-ray Diffraction Screening Method for detection of silicates in water X-ray diffraction abroad How to Quantitatively Analyze X-ray Diffraction Quantitative Analysis Method of X-ray Diffraction Analytical method derivatization x-ray diffraction radiation How to Quantitatively Analyze X-ray Diffraction x-ray analysis How to use x-ray diffraction electron diffraction phase Mini X-ray Diffraction Ray analysis Relative intensity of diffraction peaks Crystalline X-ray Diffraction Ray Diffraction X-ray diffraction peak at 27 degrees X-ray diffraction parameters X-ray diffraction analysis X-ray diffraction peak width x-ray diffraction and x-rays Powder X-ray Diffraction Analysis Quantitative analysis by x-ray diffractometer Quantitative Analysis of Ray Diffraction X-ray diffractometry Diffraction and Transmission edx x-ray analysis xrd x-ray diffraction X-ray Diffraction of Silica cement clinker Quantification by x-ray diffraction analysis How to Quantify by X-ray Diffraction ray diffraction method X-ray Diffraction Structural Analysis X-ray diffraction, X-ray fluorescence X-ray Diffraction and X-ray Fluorescence second order diffraction Diffraction Semiquantitative Phase Analysis x-ray diffraction x+ ray diffraction Seven x-ray analysis Analyze x with x-ray analysis method Novel X-ray Diffraction Diffraction in English X-ray Diffraction Silica X-ray Diffraction Intermediate xrd diffraction peak single phase Automated X-ray Diffraction X-ray Diffraction Method non-diffractive surface Mineral facies portable x-ray diffraction xrd High Energy X-ray Diffraction Alloy x-ray diffraction x-ray sample preparation method x fluorescent clinker phase diffraction surface Diffraction of x-rays x-diffraction analysis X-ray Diffraction Mineral Analysis Analyzing X-ray Diffraction Spectra Transmission and Diffraction x ray ore x-ray analysis 2 X-ray Diffraction Analysis Method X-ray Diffraction Analysis Method Broadening of x-diffraction peaks Analysis of X-ray Diffraction Spectroscopy Quantitative analysis by X-ray diffractometer The principle of rays Secondary Diffraction Diffraction Spot Neutron Diffraction Peaks Diffraction half-point analysis Principles of x-rays X-ray principle High Energy X-ray Diffraction transmission diffraction Quantitative analysis by x-ray diffractometer X-ray Diffraction Powder Analysis Diffraction analysis method X-ray Diffraction Powder Analysis Polarization + Diffraction + X-ray diffraction analysis equipment X-ray diffractometer semi-quantitative analysis X-ray diffraction + quantitative analysis Ray analysis X-ray diffraction equipment Silica X-ray Diffraction Peaks x-ray X diffraction diffracted x-rays clinker X-ray phase contrast diffractive pigment What does an x-ray diffractometer analyze? X-ray Diffraction Analysis of Clay Minerals X-diffraction rays cement clinker Mineral X-ray Diffraction Identification x-ray diffraction minerals diffracted rays Calibration of x-ray diffractometer Mineral X-ray Diffraction Identification X-ray Diffraction Phase Analysis cobalt diffraction peak X-ray stress analysis and X-ray diffraction analysis Principle of Diffraction Analysis Principles of High Energy Ray Diffraction Single crystal x-ray diffractometer analysis x-ray analysis technique Ray Diffraction Pattern What does x-ray diffractometer analyze Near Field High Energy X-ray Diffraction X-ray Diffraction Analysis Silicon standard diffraction peaks X-ray diffraction method in the analysis How to analyze x-ray diffraction spectrum X-ray Diffraction Structural Analysis X+ ray diffraction analyzer Diffraction data Second order diffraction and first order diffraction x-ray diffraction size X-ray diffractometer test method X-ray Diffraction Analysis Spectrum Diffraction x-ray absorptiometry X-ray fluorescence analysis and X-ray diffraction analysis Out-of-Plane Diffraction In-Plane Diffraction x-ray diffraction half width Molybdenum diffraction peak X-ray diffraction amorphous peak Diffraction peaks of water x-ray diffractometer How X-ray Diffraction Analyzes Phase Structure x-ray diffraction scan Powder X-ray Diffraction Analysis xrd Derivative analysis method Diffraction peaks of x-diffraction silicon X-ray diffraction peak width First Order Diffraction Second Order Diffraction What kind of rays are used in x-ray diffraction X-ray Diffraction Analysis Crystal Orientation What is x-ray diffraction used for? Diffraction plate cobalt diffraction peak X-ray Diffraction Analysis Structure Principles of X-ray Analysis x-ray tomography How to quantitatively analyze x-ray diffractometer Diffraction concept X-ray Diffraction Analyzer Diffraction peaks of silicon X-ray Diffraction Microscopic Diffraction peak position of silicon x-ray tomography X-ray principle? X-ray diffraction equipment X-ray Diffraction Mineral Identification Pearl Powder X-ray Diffraction Analysis Pearl Powder Identification Method X-ray Diffraction Analysis How is diffraction graded X-ray diffraction sample preparation volume X-ray diffraction peak position Secondary Diffraction Analysis X-ray diffraction equipment Intensity of x-ray diffraction peaks Si diffraction peak Accessory Mineral X-ray Diffraction Principles of X-ray Analysis three-point diffraction x ray and water X-ray Spectroscopy Phase Analysis X-ray Diffraction Analysis Analysis of X-ray Diffraction Peaks Mine x X-ray diffraction peak broadening x-ray principle x-ray fluorescence analysis and x-diffraction Portland cement clinker X-ray diffraction lines X-ray diffractometer qualitative analysis phase X-ray Diffraction Analysis 05 x-ray sample preparation method X-ray Diffraction Analysis Structure x-ray diffraction method x-ray diffraction and Ray Ray Analysis Diffraction double diffraction method X-ray Diffraction Analysis x analysis principle Principles of X-ray Diffraction hand-held x-diffraction X-ray diffraction peak broadening cement mine edx analysis x-ray Powder X-ray Diffraction Analysis x-ray analysis method What does x-ray diffraction measure? How about x-diffraction analysis Pigment X-ray Diffraction X-ray diffractometer analysis x-ray stress analysis X-ray diffraction structure analysis GB/T 40407-2021 x-ray camera GBT40407 GB/T 40407-2021 Cement clinker content Whole Rock X-ray Diffraction Whole-rock X-ray diffraction Rays Single Crystal X-ray Diffraction Analysis Whole-rock X-ray diffraction analysis Rock X-ray Diffraction Analysis Principle of x-ray diffractometer xrd map Silicon diffraction peak position Laue method x-ray diffraction mobile phase salt precipitation Factors affecting x-ray diffraction peaks X-ray diffraction micro analysis How to analyze x-ray diffraction patterns Characteristics of x-ray diffraction analysis X-ray diffraction analysis experimental parameter selection diffraction method Cement clinker additives Silicate detection method in water silicate mineral fluorine The linearity of the liquid phase analysis method does not meet the requirements Diffraction analysis sampling Single crystal diffraction analysis method Acceptance method for analyzing mercury hydrochloric acid Silane derivatization method

《GB/T 40407-2021硅酸盐水泥熟料矿相X射线衍射分析方法》由TC184（全国水泥标准化技术委员会）归口，主管部门为中国建筑材料联合会。

Introduction

Technical background and evolution of the standard

This standard is the first special analysis method standard for silicate cement clinker established in my country, which solves the technical bottleneck that traditional chemical analysis methods cannot distinguish isomorphous and heteromorphic crystals. After ISO released the "Cement Test Methods - Quantitative X-ray Diffraction Analysis" in 2008, my country carried out a 13-year method verification based on the Rietveld full spectrum fitting technology, and finally formed this standard.

Analysis of core analysis methods

Analysis dimension	Traditional method	This standard method
Resolution	Single peak analysis (0.5° step width)	Full spectrum fitting (0.02° step width)
Accuracy	Relative error ≥15%	Alite phase error ≤3%
Applicable phase	Main crystal phase	Can distinguish M1/M3 crystal forms of C3S

Typical Application Cases

A cement plant found abnormal belite content when testing clinker with a Rigaku SmartLab diffractometer. Through the Rietveld refinement of Clause 6.6 of this standard, it was found that it was caused by the conversion of β-C2S to γ-C2S. After adjusting the calcination system, the 28-day strength was increased by 4MPa.

Key Implementation Points

Instrument calibration cycle: The goniometer angle must be calibrated with silicon powder standard material every 6 months, and calibration is required immediately after replacing the X-ray tube
Sample preparation: When the powder is ground to less than 45μm, the preferred orientation error can be controlled within 2%
Data validity: Rwp＜8% and the range of three parallel measurements meets the requirements of Table 1

Radiation Safety Management

The standard places special emphasis on radiation protection of the diffractometer, and requires:

Workplace dose rate ≤2.5μSv/h
Be filter must be installed on the X-ray tube window
Emergency stop button response time ＜0.5 seconds

Technology Development Outlook

With the application of synchrotron radiation light sources, the detection limit may be increased from the current 1% to 0.1% in the future, and real-time monitoring of the free state of CaO can be achieved. This standard lays the foundation for subsequent high-precision analysis methods.

More samples: JC/T 2453-2018 JGJ 94-2008 QC/T 942-2021

Sample only — not a preview of GB/T 40407-2021

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