GB/T 5009.74-2003 in English
SUPERSEDEDMethod for limit test of heavy metals in food additives
- Issued on:2003-08-11
- Implemented on:2004-01-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
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《GB/T 5009.74-2003食品添加剂中重金属限量试验》由361(国家卫生健康委员会)归口,主管部门为国家卫生健康委员会。
本标准规定了食品添加剂中重金属的限量试验方法。本标准适用于食品添加剂中重金属的限量试验。
Method for Limit Test of Heavy Metals in Food Additives
1 Scope
This standard specifies the method for limit test of heavy metals in food additives.
This standard is applicable to the limit test of heavy metals in food additives.
2 Principle
In the presence of weak acid (pH 3~4), heavy metal ion in the test sample will act with hydrogen sulfide to generate a substance in brownish black, which is compared to the lead standard solution experiencing the same treatment for limit test.
3 Reagents
3.1 Nitric acid.
3.2 Sulfuric acid.
3.3 Hydrochloric acid.
3.3.1 6 mol/L hydrochloric acid: measure 50mL of hydrochloric acid and dilute it with water to 100 mL.
3.3.2 1 mol/L hydrochloric acid: measure 8.3mL of hydrochloric acid and dilute it with water to 100 mL.

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