GB/T 34172-2017 in English
VALIDMicrobeam analysis--Electron backscatter diffraction--Phase analysis method of metal and alloy
- Issued on:2017-09-07
- Implemented on:2018-08-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
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《GB/T 34172-2017微束分析 电子背散射衍射 金属及合金的相分析方法》由TC38(全国微束分析标准化技术委员会)归口,主管部门为国家标准化管理委员会。
Introduction
National Standard of the People's Republic of China GB/T 34172—2017
Microbeam Analysis Electron Backscatter Diffraction Phase Analysis Method for Metals and Alloys
Introduction
Electron backscatter diffraction (EBSD) is an analysis method based on the electron beam in a scanning electron microscope (SEM) or a focused ion beam (SEM-FIB) exciting backscattered electrons on the inclined sample surface and diffracting through the surface atoms of the sample to form Kikuchi bands. This technology is widely used in the study of crystal structure, phase distribution and orientation relationship of metal and alloy materials.
GB/T 34172—2017 standard provides unified technical specifications for the application of EBSD in metals and alloys, including parameter correction, data acquisition and analysis methods.
Scope of application
- Applicable to the phase qualitative and quantitative analysis of metal and alloy samples by EBSD technology.
- Standardizes parameter calibration and data acquisition methods to ensure the accuracy and reliability of the results.
- EBSD phase analysis of other polycrystalline or single crystal materials can be performed for reference.
| Standard dimensions | GB/T 34172—2017 requirements | International comparison |
|---|---|---|
| Sample preparation | The surface is flat and clean, without deformation layer and oxidation pollution. | Consistent with international standard requirements. |
| Accelerating voltage range | 15~30 kV | In line with the international recommended range. |
| Step size selection | It is recommended to take 1/10 of the average grain size of the sample. | Similar to ASTM standard. |
Implementation suggestions
1. Parameter optimization:Adjust the accelerating voltage, beam current and working distance according to the characteristics of the sample to ensure data quality.
2. Data acquisition:Preferably use high-quality CCD pixel integration (such as 1×1 or 2×2) to improve the resolution of the diffraction pattern.
3. Background correction:Use low-magnification rapid scanning to obtain background information to ensure the quality of EBSP.
4. Quantitative analysis:Combined with EDS/WDS element analysis results, the reliability of phase identification is improved.
Conclusion
GB/T 34172—2017 provides comprehensive technical specifications for the application of EBSD technology in metals and alloys, and clearly defines the requirements for the entire process from sample preparation to data processing. Following this standard can effectively improve the accuracy and consistency of phase analysis results.
It is recommended to optimize parameter settings in combination with specific material properties in actual operation, and to ensure system stability by regularly calibrating the equipment.

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