GB/T 24582-2009 in English
SUPERSEDEDTest method for measuring surface metal contamination of polycrystalline silicon by acid extraction-inductively coupled plasma mass spectrometry
- Issued on:2009-10-30
- Implemented on:2010-06-01
- File Format:PDF
- Delivery:Via email within 1~3 business days
$117.00
《GB/T 24582-2009酸浸取 电感耦合等离子质谱仪测定多晶硅表面金属杂质》由TC203(全国半导体设备和材料标准化技术委员会)归口,TC203SC2(全国半导体设备和材料标准化技术委员会材料分会)执行,主管部门为国家标准化管理委员会。
本标准规定了用酸从多晶硅块表面浸取金属杂质,并用电感耦合等离子质谱仪定量检测多晶硅表面上的金属杂质痕量分析方法。
本标准适用于碱金属、碱土金属和第一系列过渡元素如钠、钾、钙、铁、镍、铜、锌以及其他元素如铝的检测。
本标准适用于各种棒、块、粒、片状多晶表面金属污染物的检测。由于块、片或粒形状不规则,面积很难准确测定,故根据样品重量计算结果,使用的样品重量为50g~300g,检测限为0.01ng/mL。
Scope
This standard specifies the analysis method for leaching metal impurities from the surface of polycrystalline silicon block with acid, and quantitatively detecting the trace amount of metal impurities on the surface of polycrystalline silicon with inductively coupled plasma mass spectrometer. This standard applies to the detection of alkali metals, alkaline earth metals and the first series of transition elements such as sodium, potassium, calcium, iron, nickel, copper, zinc and other elements such as aluminum. This standard applies to the detection of metal contaminants on the surface of various rods, blocks, grains, and flakes. Due to the irregular shape of blocks, flakes or granules, it is difficult to accurately measure the area. Therefore, according to the calculation results of the sample weight, the sample weight used is 50 g to 300 g, and the detection limit is 0.01 ng/mL. The concentration, composition, temperature and leaching time of the acid determine the depth of surface corrosion and the leaching benefit of surface contaminants. Less than 1% of the sample weight was etched away in this experimental method. This standard applies to the determination of samples with a weight of 25 g to 5000 g. In order to achieve the purpose of arbitration, this test method stipulates that the weight of the sample is about 300 g.

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