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JY/T 0584-2020 in English

JY/T 0584-2020 in English

VALID

General rules of analytical methods for scanning electron microscope

  • Issued on:2020-09-29
  • Implemented on:2020-12-01
  • File Format:PDF
  • Delivery:Via email within 1~3 business days
Price(USD): $250.00
$243.00
Standard No: JY/T 0584-2020
Document status: VALID
Title in English: General rules of analytical methods for scanning electron microscope
Title in Chinese: 扫描电子显微镜分析方法通则
Language: English
File Format: Electronic (PDF)
Delivery: Via email within 1~3 business days
Issued on: 2020-09-29
Implemented on: 2020-12-01
Superseding: JY/T 010-1996 General rules for analytical scanning electron microscopy
Professional Classification: JY-Education
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Use of Scanning Microscopes
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When using a scanning electron microscope
SEM fiber analysis
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Scanning Electron Microscope Main Observation
Environmental Field SEM
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The work of the scanning electron microscope
SEM below 10
Environmental Field SEM
Scanning Electron Microscopy
SEM sample preparation method
Scanning Microscopes and Electron Microscopes
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Environmental Field Scanning Electron Microscopy
SEM analysis of particles
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Scanning Electron Microscopy Spectroscopy
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JY/T 0567-2020
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ultra high voltage electron microscope
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Introduction

Analysis of the core content of the standard

Technical modules Contents of the 1996 version Additions/modifications to the 2020 version
Terminology 12 basic terms 8 new key technical terms such as Environmental scanning electron microscope and Cathode fluorescence
Instrument configuration Basic SEM functions Added technical specifications for Electron backscatter diffractometer and Cathode fluorescence system
Sample Preparation General Sample Preparation Methods New Special Preparation Requirements for Spectroscopy Test and EBSD Samples

Detailed Explanation of Key Technical Points

4.1 Imaging Mode Selection Matrix

Imaging Mode Applicable Samples Resolution Range Typical Applications
Secondary Electron Image Surface Morphology Analysis 1-10nm Material Fracture Analysis, Biological Samples
Backscattered electron image Composition contrast analysis 10-50nm Alloy phase distribution, mineral identification
Cathode fluorescence image Semiconductor materials 100-500nm Defect location, energy band analysis

5. Laboratory environment control indicators

  • Temperature and humidity control: 20±5℃, humidity ≤75%
  • Electromagnetic interference: ≤5μT alternating magnetic field
  • Vibration control: foundation amplitude ≤5μm (5-20Hz)

Recommendations for the implementation of the standard

Typical application cases

A scientific research institution used a field emission scanning electron microscope in conjunction with an EBSD system to analyze the grain boundary characteristics of titanium alloy:

  1. Electrolytic polishing was performed according to Clause 7.3.3
  2. The working distance was set to 15mm, and the accelerating voltage was 20kV
  3. Orientation contrast images were acquired using a 4-segment backscatter detector
  4. Scanning step size was 0.1μm, and the acquisition speed was 300 points/second

Instrument selection reference

Electron gun type Resolution (nm) Applicable scenarios
Tungsten filament 4 General material analysis
Field emission 1 Nanomaterial research

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